ProcessLab ADI 2045PL Robust at-line analyzer for process analysis ProcessLab ADI 2045PL – the innovative solution for routine analysis in production 02 The ProcessLab ADI 2045PL is by far the most robust On-line or at-line? routine system for at-line ion analysis on the production The infrastructure and costs to facilitate on-line analysis floor and in control Labs. Metrohm Applikon’s 40 years can be high especially when multiple sampling points are experience with on-line analysis resulted in a new system to be considered. Difficult sampling and complicated for custom made at-line process analysis. The ProcessLab sample preparation can also be limiting factors to con-ADI 2045PL guarantees the highest level of reliable ana-nect the analyzer on-line. In cases like this, installation of lytical results. The new additional ProcessLab Manager a ProcessLab ADI 2045PL at-line analyzer can be a very software offers a user-friendly interface in combination cost-efficient solution: Samples are taken manually at with the tiamo TM laboratory software. each sampling point, fed into the ProcessLab ADI 2045PL (manually or by means of an autosampler), and automatically analyzed. In this way different samples from various process stages can be cost-efficiently analyzed on a single system. 03 The ProcessLab ADI 2045PL offers ... • simple operation due to graphical user interface • robust hardware IP66/NEMA 4 • complete separation of wet part and electronics • modular and maximum flexibility for every application • Touch Screen: Industrial PC with 15” TFT • ethernet TCP/IP Network for remote control and data storage • 20 wet parts for maximum space of analytical modules • leak and level detection for reagent and waste containers • analog outputs/inputs for results and process control • USB connection (external/internal) for storage and method transfer Analysis methods – versatility at your fingertips 04 The ProcessLab ADI 2045PL is programmed for one or Moreover, data from third-party devices such as more of the following methods and adapted to specific analysis re quirements. • Density • Temperature • Titration for a broad range of applications • Flow, turbility • Karl Fischer titration for water determination • Conductivity, etc. (oil, solvents, glycol, ...) • Photometry for water quality analysis & various can be imported through the analog input channels for plating solutions correcting results and providing added monitoring value. • Standard addition for ion specific analysis that uses Ion Selective Electrodes The capability to choose a combination of methods means • Direct measurement for measuring physical para-that in most cases a single ProcessLab ADI 2045PL will meters such as pH, conductivity and temperature fulfil all analysis requirements. Furthermore, the op tion for simultaneous analysis to increase response times makes the ProcessLab ADI 2045PL an even more power-ful at-line analyzer. Examples of typical applications Thanks to Metrohm’s many years of experience in the As a result of the high flexibility of the individual mo-field of ion analysis, we are able to measure numerous dules, the ProcessLab ADI 2045PL is highly versatile. Ty pi-analytical parameters, of which the following are parti- cal application fields are listed below: cularly important in process analysis: Etching baths in the steel industry • pH value Determination of the content of acids and metals in etch- • Conductivity ing baths. • Redox potential • Acid content Semiconductor / Solar • Free and total alkalinity Determination of mixed acid etchants • Water hardness • Phosphates Baths in the electroplating industry • Chloride Typical parameters in electroplating baths including the • Chlorine cleaning and degreasing baths used for pretreatment. • Ammonia • Nitrite Phosphating baths in the automobile industry • Fe, Cu, Ni, Zn All the important parameters for monitoring a complete • Na, Ca, F (with ISE) Phosphating plant. • Free and total SO2 • Sulfate Process baths in the paper industry • H S/mercaptans Parameters in the cooking liquor or the so-called white, 2 • Hydrogen peroxide green or black liquors in the paper industry. • Free fatty acids • Surfactants Parameters in the food industry • Water content Important parameters for the quality control of food- • Organic additives (CVS) stuffs, for example in instant soups or fruit juices. All analytical methods that are already used in the lab can Applications for automated sample preparation easily be transferred to process analysis. For example special projects requiring liquid handling for automatic dilution, extraction, and filtration. Modularity for maximum flexibility 06 The ProcessLab ADI 2045PL uses high-quality Metrohm ronments. The industrial housing separates the electron-analysis modules. In combination with Applikon’s experi-ics from the wet part. Any combination of burettes, ence in process control instrumentation this results in an pumps, vessels, loops, etc. is possible, enabling hundreds at-line analyzer that performs in the most difficult envi-of functional layouts. AgNO3 MIX MOLYBDATE H2O DILUTION H2SO4 & AgSO4 MOHR's SALT mV REF-DJ ACID CARRIER AIR K2Cr2O7 & Hg 5 ml/min 5 ml/min 40 ml/min A A A A 20 ml 20 ml 10 ml 10 ml 10 ml 10 ml EARTH pH REF mV Ref DJ A A A A A A in out in out in out CARRIER HNO3 [1 M] CARRIER 40 ml/min 40 ml/min 40 ml/min 10 ml A A A in out in out in out 40-150 ml 5-70 ml 40-150 ml NH3 [5%] 40 ml/min out carrier in out carrier in X ML 3 3 out sample in out sample in RINSE in out loop volume loop volume SAMPLE 1 ML 0,5 ML SAMPLE [A] RINSE DRAIN SAMPLE [B] RINSE DRAIN 40 ml/min 120 ml/min 120 ml/min 40 ml/min 320 ml/min 320 ml/min VENT COOLER in out in out in out in out DRAIN RINSE AIR DRAIN RINSE in out in out SAMPLE DRAIN Examples of possible layouts for the wet-chemistry part of the analyzer 07 Countless combinations possible The ProcessLab ADI 2045PL is set up according to the analysis modules. This results in simply structured and user’s specific requirements. Each analysis module con-clearly laid-out analysis units. Sample introduction can be tains exactly those components that are required for the performed manually or more conveniently by means of analysis to be carried out. A wide range of analytical a Sample Processor when higher throughput is required. systems can be configured by the combination of several The software – freely programmable and user-defined 08 The ProcessLab ADI 2045PL can be programmed and interface. Users just have to press a Start button icon on controlled in two different ways using either the well-the touch screen or use the Remote Start option to start proven tiamo TM software or the ProcessLab Manager the analysis. (PLM) package. tiamo TM may be preferred by users al - ready experienced with this software in the laboratory. The ProcessLab ADI 2045PL can also be remotely con-The PLM software offers a user-defined flexible shell on trolled using Teamviewersoftware via the Ethernet. top of tiamo TM for a very clear and easy-to-use graphical 09 Networking and process integration The digital and analog input/output (I/O) components ProcessLab ADI 2045PL can also be easily integrated in a available allow the system to be very easily integrated in local network or be fully operated by remote control. the process environment. In this way the system can react Analysis data can be exported to any LIMS or made avail-to different input signals and commands, for example able to a process control system. automatically measure different parameters depending on the sample, trigger an alarm if limits are exceeded or transmit measured values using 4-20 mA analog output signals. I/O controller remote maintenance control inputs/outputs local network local network evaluation remote control Comprehensive communication possibilities Specifications ProcessLab ADI 2045PL 10 Applied Analysis Methods Connectivity ADI 2045PL Titration Data Communication Ethernet: TCP/IP network Karl Fischer titration serial interface, USB 2.0 Photometry Analog Output 4 x 4-20 mA per I/O terminal Standard addition with (multiple I/O terminals possible) ion-selective electrode Analog Input 2 x 4-20 mA or 0-2 V per Direct measurement of pH, I/O terminal mV, conductivity, temperature (multiple I/O terminals possible) Digital Output 4 x 24 VDC per I/O terminal Sampling Batchwise or Frequency Programmable 2 x 12-230 VAC per I/O terminal Streams Multiple (multiple I/O terminals possible) Volume 0.1-100 ml Relay Output 2 x Potential free relay per Temperature 5-90 °C / 41-194 F I/O terminal Pressure 0-4 bar / 0-72 PSI (multiple I/O terminals possible) (without preconditioning) Digital Input 4 x 24 VDC per I/O terminal (multiple I/O terminals possible) General Power Supply 100-120 / 200-240 V / 690 VA / 50...60 Hz Housing Material Standard: «electronics cabinet»: zinc plated steel, epoxy coated «Wet Part» door: polystyrene, epoxy coated Optional: stainless steel SS316 Ingress Protection IP66/NEMA 4 Ambient Temperature 5-40 °C Dimensions H x W x D 870 x 700 x 510 mm Weight ~75 kg Accessibility Passcode protected Any doubts if on-line is the way to go? Start at-line and upgrade to on-line Selection of most commonly used options 11 The ProcessLab ADI 2045PL can be easily upgraded to an • Level detectors Process Analyzer ADI 2045TI for on-line analysis. Simply • Reagent cabinet with level detectors start with the ProcessLab ADI 2045PL at-line and up - • Ethernet connection grade to on-line to gain the maximum on savings with • Pneumatic Actuators (valves, ...) complete process automation. Installation of software • Digital and analog inputs and outputs and a by-pass connection to the process is all that is required to start analyzing on-line. Downgrading any Please contact your local Metrohm distributor for the Metrohm Applikon on-line ana lyzer to an at-line system pre cise configuration and setup of the Pro cess Lab ADI is also possible. 2045PL. Thanks to the modularity, the system allows on-site adaptation to any individual requirements. ➡ ➡ Processlab ADI 2045PL with stand on a table For further information, consult www.metrohm-applikon.com www.metrohm.com witzerland G, CH-9100 Herisau, S ohm A , printed by Metr SW Subject to change without prior notice Layout by Ecknauer+Schoch A 8.000.5078EN – 2012-06