2018/2019 Metrohm Autolab Microcell HC & Accessories Catalogue Electrochemistry with temperature control • Systems • Cel s • Software • Accessories © 2013-2018 RHD Instruments GmbH & Co. KG Features are subject to change without notice. Unlabeled images are example images il ustrating the product category or product type. Actual products may vary. Plots are used with the permission of rhd Instruments. Content Autolab Microcel HC - Basic Package Autolab Microcell HC Basic Package closed 03 Autolab Microcell HC Basic Package open Autolab Microcell HC - Measuring Cel s TSC 70 Open 04 TSC 1600 Open 05 TSC Sw Open 06 TSC 70 Closed 07 TSC 1600 Closed 08 TSC Sw Closed 09 TSC Battery standard/expanded 10 TSC Surface 11 TSC Spectro 12 Autolab Microcel HC - Software NOVA 2 13 RelaxIS Autolab Microcell HC - Accessories O-rings 14 Heat sink compound Cleaning and polishing set Diamond paste 0.25 μm Conductivity standard solution 15 rhd Cooling box Serial connection kit Adapter box BNC/banana plug or BNC/BNC Cap with 4 glass-sealed Pt electrodes 16 Electrode plug with 4 glass-sealed Pt electrodes Cap with exchangeable electrode Micro reference electrode classical 17 Micro reference electrode ionic liquid Micro reference electrode organic carbonate 18 Micro reference electrodes pseudo Mount for Li-reference electrode 19 Stainless steel disc electrodes Stainless steel disc electrodes gold plated Nickel disc electrodes Nickel disc electrodes gold plated Stainless steel disc electrodes nickel plated Spacer set Capillary-based filling set 20 Content Capil ary-based gas-inlet set Cable feed-through, with 40 mm DIN flange Faraday cage Faraday cage with dew point sensor Modification set item no. 101 to 102 21 Passive cell holder Modification set item no. 102 to 101 100 Ohm Test resistor Transport case Autolab Microcell HC - Spare parts and consumables O-rings 22 Spare parts for TSC 70 closed 23 Spare parts for TSC 1600 closed 24 Spare parts for TSC battery 25 Spare parts for TSC surface 28 Spare parts for TSC spectro 30 Autolab Microcell HC - Basic Package Item 101 - Autolab Microcell HC Basic Package closed 03 Basic setup, compatible with all closed measuring cells. Included: • 1 Cell holder Autolab Microcell HC • 1 temperature controller 3216 • 1 heat sink compound (Item 411, page 14) • 1 Serial connection kit (item no. 441) • 1 Adapter box BNC - banana (item no. 442) • All required connection cables + tools No measuring cell included. Temperature controller Cel holder Item 102 - Autolab Microcell HC Basic Package open Basic setup, compatible with all open measuring cells. Included: • 1 Cell holder Autolab Microcell HC • 1 Positioning unit with micrometer screw (item no. 572) • 1 temperature controller 3216 • 1 heat sink compound (Item 411, page 14) • 1 Serial connection kit (item no. 441) • 1 Adapter box BNC - banana (item no. 442) • All required connection cables + tools No measuring cell included. Temperature controller Cel holder Autolab Microcell HC - Measuring Cel s 04 Item 201 - TSC 70 open Measuring cell - type open for liquid samples Specifications: • For liquid samples • V = 70 μL, V = 100 μL min max • Electrode diameter (Pt wire): 0.25 mm each • T-range (operation): -40 °C to +100 °C, depending on sample’s mass and humidity conditions • T-range (storage): +10 °C to 30 °C Included: • 1 Cell unit with Pt sample container • Electrode plug with 4 glass-sealed Pt wires (item no. 511) Selected applications: • Determination of dc-ion conductivity of ionic liquids and other non-volatile ‘liquid’ samples like polymerized ionic liquids • Determination of the electrochemical window of ionic liquids (only with internal Pt pseudo-reference electrode of electrode plug) Electrode plug Sample container Autolab Microcell HC - Measuring Cel s 202 TSC 1600 open 05 Measuring cell - type open for liquid samples Specifications: • For liquid samples • V = 1.0 mL, V = 1.2 mL min max • Electrode diameter (Pt wire): 0.25 mm each • T-range (operation): -40 °C to +100 °C, depending on sample’s mass and humidity conditions • T-range (storage): +10 °C to 30 °C Included: • 1 Cell unit with Pt sample container • 1 Electrode plug with 4 glass-sealed Pt wires (item no. 511) Selected applications: • Determination of dc-ion conductivity of ionic liquids and other non-volatile ‘liquid’ samples like polymerized ionic liquids • Determination of the electrochemical window of ionic liquids (only internal Pt pseudo-reference electrode of electrode plug) Temperature dependent cyclic voltammetry plots Electrode plug Sample container Autolab Microcell HC - Measuring Cel s 06 Item 203 - TSC Sw open Measuring cell - type open Specifications: • Maximum diameter of disc-shaped samples (solid): 12mm • Samples are ideally disc-like in shape and dimensionally stable when being set under pressure • T-range (operation): -40 °C to +100 °C, depending on sample’s mass and humidity conditions • T-range (storage): +10 °C to 30 °C Included: • 1 Electrode plug with one-sided polished stainless steel disc (diameter: 12 mm) • 1 Cell unit containing one exchangeable one-sided polished stainless steel disc electrode for sample mounting • 1 Cover made of PEEK to simplify positioning of the upper electrode Selected applications: • Determination of dc-ion conductivity of gels and glasses • Dielectric spectroscopy of solid samples Electrode plug Arrhenius plot Sample mount equipped with Disc electrode with cover and disc electrode spherical joint Autolab Microcell HC - Measuring Cel s Item 211 - TSC 70 closed 07 Measuring cell - type closed Specifications: • For liquid samples • V = 70 µL, V = 100 µL min max • Electrode diameter (plug): 0.25 mm each • T-range (operation): -40 °C to +100 °C, depending on sample’s mass and humidity conditions • T-range (storage): +10 °C to 30 °C Included: • 1 Cell unit with Pt sample container • 1 Cap containing electrode plug with 4 glass-sealed Pt wires and two plugs which seal two inlets for connecting fittings (item no. 501) • 1 Cover made of PEEK • 2 O-rings 15 x 2 mm made of EPDM by default; other materials are available (item no. 401) Selected applications: • Determination of dc-ion conductivity of liquid volatile and/or moisture and air-sensitive samples like carbonate-based battery electrolytes or dye solutions in organic solvents like acetonitrile Cap with electrode plug • Determination of the electrochemical window of liquid volatile and/or moisture and air-sensitive samples - several capil ary-based reference electrodes as well as mountings for Li pseudo-reference electrodes are available (item no. 5241, 525, 5261 and 5271) Sample container with PEEK cover Assembled Autolab Microcell HC - Measuring Cel s 08 Item 212 - TSC 1600 closed Measuring cell - type closed Specifications: • For liquid samples • V = 1.0 mL, V = 1.2 mL min max • Electrode diameter (plug): 0.25 mm each • T-range (operation): -40 °C to +100 °C, depending on sample’s mass and humidity conditions • T-range (storage): +10 °C to 30 °C Included: • 1 Cell unit with Pt sample container • 1 Cap containing electrode plug with 4 glass-sealed Pt wires and two plugs which seal two inlets for connecting fittings (item no. 501) • 1 Cover made of PEEK • 2 O-rings 15 x 2 mm made of EPDM by default; other materials available (item no. 401) Selected applications: • Determination of dc-ion conductivity of liquid volatile and/or moisture and air-sensitive samples like carbonate-based battery electrolytes • Determination of HOMO-LUMO gaps of organic dyes by measuring cyclic voltammograms of dye solutions in Cap with electrode plug organic solvents like acetonitrile • Determination of the electrochemical window of liquid volatile and/or moisture and air-sensitive samples - several capillary-based reference electrodes as well as mountings for Li pseudo-reference electrodes are available (item no. 5241, 525, 5261 and 5271) Sample container with PEEK cover Assembled Autolab Microcell HC - Measuring Cel s Item 213 - TSC Sw closed 09 Measuring cell - type closed Specifications: • Max. diameter of disc-shaped samples (solid): 12 mm • Samples are ideally disc-like in shape and dimensionally stable when being set under pressure • T-range (operation): -40 °C to +100 °C, depending on sample’s mass and humidity conditions • T-range (storage): +10 °C to 30 °C Included: • 1 Cell unit containing one exchangeable one-sided polished stainless steel disc electrode for sample mounting • 1 Cover made of PEEK • 1 ball joint-fixed pollished stainless steel disc electrode for contacting sample or current collector • 1 Gold-plated spring for pressure adjustment • 1 Cap with spring contact • 2 O-rings 15 x 2 mm made of EPDM by default; other materials are available (item no. 401) Selected applications: • Determination of dc-ion conductivity of gels and glasses • Dielectric spectroscopy of solid samples Cap with spring contact Measuring cell without cap Platform for sample mounting Autolab Microcell HC - Measuring Cel s 10 Item 214_s/e - TSC battery standard/expanded Measuring cell - type closed Specifications: • Maximum diameter of disc-shaped solid sample: 12 mm • Samples are ideally disc-like in shape and dimensionally stable when being set under pressure • T-range (operation): -40 °C to +100 °C, depending on sample’s mass and humidity conditions • T-range (storage): +10 °C to 30 °C Cap with spring contact Included: • 1 Nickel-plated cell unit to fix lower electrode • 2 Stainless steel electrodes (pressed in PEEK) for flat samples • 2 Electrodes* (pressed in PEEK) for usage of elemental lithium. Electrode material is stainless steel • 1 Cover made of PEEK Gold-plated spring • 1 Gold-plated spring and screw • 1 Cap with spring contact • 3 Screw plugs: Li reference plug, capillary plug and blank plug • O-rings: 4 (8)* x item no. 402 EPDM, 2 x item no. 405 EPDM, 3 x item no. 406 FFKM) Gold-plated screw • 100 Ohm test resistor (item no. 591) Selected applications: • Determination of dc-ion conductivity of solid ion conductors, glasses, and gels Upper electrode • Dielectric spectroscopy of solid samples • Investigations of batteries (half and full cells) and super-caps in two or three-electrode configuration • Determination of MacMullin number (separators) • Studies of hybrid materials (solid + liquid) Lower electrode for flat sample Screw plug for capillaries Assembled * Only included in the expanded version Autolab Microcell HC - Measuring Cel s Item 215 - TSC surface 11 Measuring cell - type closed Specifications: • Rectangular solid samples: minimum side length: 10 mm, maximum side length: 15 mm • Round solid samples: minimum diameter: 12 mm, maximum diameter: 20 mm • Maximum sample thickness: 2mm • Samples should be dimensionally stable when being set under pressure • T-range (operation): -40 °C to +100 °C, depending on Cap with exchangeable sample’s mass and humidity conditions glassy carbon electrode • T-range (storage): +10 °C to 30 °C Included: • 1 Gold-plated platform for sample mounting Screw plug for capillaries • 1 Cover made of PEEK containing 4 gold-plated contact springs • 1 Cap with exchangeable glassy carbon electrode (diameter: 6 mm; item no. 510, short) • 3 Plugs: Li reference plug, capillary plug and blank plug • O-rings: 1 x item no. 401 EPDM, 2 x item no. 404 FFKM, 3 x item no. 406 FFKM) Selected applications: PEEK cover with four • Corrosion studies contact pins • Investigation of the electrochemistry of solid/liquid interfaces Platform for sample mounting Nyquist plot Assembled Autolab Microcell HC - Measuring Cel s 12 Item 216 - TSC spectro Measuring cell - type closed Specifications: • For liquid samples • V = 0.5 mL*, V = 2.0 mL min max • Working electrode: Pt gauze electrode by default • Counter electrode: glassy carbon (cap with exchangeable electrode) Cap with exchangeable electrode • 2 Windows equipped with collimator lenses enable UV/Vis measurements in transmission mode • Optical path length adjustable: ~1.4 mm to 0.12 mm (thickness of Pt mesh) • Wavelengths: 200-2500 nm • T-range (operation): -20 °C to +80 °C, depending on sample’s mass and humidity conditions • T-range (storage): +10 °C to 30 °C Included: • 1 Gold-plated platform for working electrode mounting Light-proof PEEK cover with • 1 Pt gauze electrode optical windows • 1 Cap with exchangeable glassy carbon electrode (item no. 512, long); on demand: item no. 510 (short) • 1 Light-proof PEEK cover Pt gauze electrode • 2 Screw plugs: capillary plug and blank plug • O-rings: 2 x item no. 401 FFKM, 1 x item no. 402 FFKM, 1 x item no. 404 FFKM, 1 x item no. 406 FFKM, 2 x 407 FFKM Selected applications: • Spectroelectrochemical studies of inorganic metal com-plexes or organic dyes in solution (CV + UV/Vis) Bottom view of PEEK housing Gold plated platform Assembled * in combination with SP 5102 Autolab Microcel HC - Software NOVA 2 Software 13 NOVA is the control software for all Autolab instruments and has built-in temperature control and measurement. Temperature control can be integrated into any electrochemical procedure. Convenient export of EIS data for analysis with rhd RelaxIS software. System Requirements • Microsoft Windows 7 or later • .NET Framework 4.5 or above Item 311 - RelaxIS* Stand alone fitting software with training option (simulation). Single license with unlimited validity period. The software can be installed on an unlimited number of computers but can only be used by one computer at a time. Included: • 1 Licence for one PC (unlimited number of users) • Service and support System Requirements • Microsoft Windows Vista (SP2) or above • .NET Framework 4.5 or above * Please check with your Metrohm distributor for availability. Impedance spectroscopy analysis Autolab Microcel HC - Accessories 14 Item 401x -407x - O-rings Item No. Size EPDM FKM FFKM 04 x 1.0 mm 406E 406F 406FF 05 x 1.0 mm - - 407FF 06 x 1.5 mm 404E 404F 404FF 07 x 1.5 mm 403E 403F - 10 x 1.0 mm 402E - 402FF 15 x 2.0 mm 401E 401F 401FF 17 x 2.0 mm 405E - - Amount: FFKM: 6 pcs. FKM/EPDM: 20 pcs. Please check the table on page 22 for the O-ring amounts and the materials included by default with the delivery for the respective measuring cell. Prior to use please check the compatibility of the respective O-ring material with all of your chemicals! Incompatibility may not only result in swelling of the O-rings, but also in serious damage to your sample and even the measuring cell. Item 411 - Servisol heat sink compound Amount: 1 ml. The Safety Data Sheet of the Servisol heat sink compound is available by request. Item 412 - Cleaning and polishing set - Option: -110 V Included: • 1 x 10 g Diamond paste (0.25 μm particle size) • 560 Cotton pads • 800 Polishing sticks • Handheld electrical multipurpose tool • 5 Polishing pads • 1 Voltage converter 110 V to 230 V (only 110 V option, e.g. for US customers) Item 413 - Diamond paste 0.25 μm Amount: 10 g. Autolab Microcell HC - Accessories Item 42x - Conductivity standard solution 15 421: sDC = 1.413 mS/cm @ 25 °C 422: sDC = 12.880 mS/cm @ 25 °C Amount: 25 pcs of 20 mL each. Item 431 - Cooling Box Cooling box needed for low temperature measurements or below dew point. Included: • Temperature controller equipped with display • Cable feed-through containing one connecting cable Autolab Microcell HC setup/temperature controller and 4 x BNC connecting cables • 1 Platform suitable for Autolab Microcell HC cell holders Important: Rated for 230 V; item no. 444 (voltage converter required for e.g. US customers). Item 441 - Serial connection kit Autolab Microcell HC setup not included Required if no native serial connection is available for communicating with the temperature controller (incl. in item no. 101/102). Included: • Moxa® USB-to-serial adapter • Driver CD Item 442 - Adapter Box BNC - Banana plug An elegant way of connecting the measuring cells and the Autolab Microcell HC set up with the Metrohm Autolab potentiostat/galvanostat and lowers the influence of interference (incl. in item no. 101 and 102). Included: • 3 x BNC cable of 30 cm length Autolab Microcell HC - Accessories 16 Item 501 - Cap (4 glass-sealed Pt electrodes) Cap containing 4 separate glass-sealed Pt- electrodes (diameter = 0.25mm each); surface mirror-like polished. Suitable for: • Item no. 211, 212 and 215 Item 502-510 Cap with exchangeable Electrode Tips (ET) Electrode Tips (ET) Cap containing: • 1 Exchangeable electrode pressed in PEEK made of various materials with diverging diameters and lengths as stated in the table on page 17; electrode surface mirror-like polished. Included: • Tool for electrode exchange (only for caps with 3 mm electrodes) + 1 x item no. 404 FFKM In case of spare parts, only the part specified in the table on page 17 is included with delivery. If the spare part is an electrode, the scope of delivery also includes 1 x item no. 404 FFKM. Stainless steel electrode, short, Ø = 6.0 mm Cap with contact pin Glassy carbon electrode, w/o electrode Ø = 3.0 mm Item 511 - Electrode plug w/4 glass-sealed Pt electrodes Electrode plug for use with open measuring cell; 4 separate glass-sealed Pt electrodes (diameter = 0.25 mm each); surface mirror-like polished. Suitable for: • Item no. 201 and 202 Autolab Microcell HC - Accessories Item No. Description Material Diameter Type Suitable for 17 (mm) measuring cell 502 Cap* Glassy carbon 3 211*, 212, (215) 5021 ET for 502 Glassy carbon 3 211*, 212, (215) 5022 ET for 502 Cap with contact pin w/o electrode 211*, 212, (215) 503 Cap Stainless steel 6 Short 215, 216 5031 ET for 503 Stainless steel 6 Short 215, 216 504 Cap* Stainless steel 3 211*, 212, (215) 5041 ET for 504 Stainless steel 3 211*, 212, (215) 505 Cap Platinum 6 Short 215, 216 5051 ET for 505 Platinum 6 Short 215, 216 506 Cap* Platinum 3 211*, 212, (215) 5061 ET for 506 Platinum 3 211*, 212, (215) 507 Cap Copper 6 Short 215, 216 5071 ET for 507 Copper 6 Short 215, 216 5081 Cap* Copper 3 211*, 212, (215) 081 ET for 508 Copper 3 211*, 212, (215) 510 Cap Glassy carbon 6 Short 215, 216 5101 ET for 510 Glassy carbon 6 Short 215, 216 5102 ET for 510 Glassy carbon 6 Long 216 *Only 2-electrode measurements are possible with item no. 211. Item no. 5022 - empty cap for 502 can be used in combination with all electrode tips. Item 521 - Micro reference electrode classical Micro reference electrode based on the system Ag/AgCl//KCl 3 M in H O. 2 Item 522 - Micro reference electrode ionic liquid Micro reference electrode based on the system Ag/AgCl//AgOTf 10 mM in [EMIm]TFSI. For items 521-23 please check with your Metrohm distributor for availability. Autolab Microcel HC - Accessories 18 Item 523 - Micro reference electrode organic carbonate Micro reference electrode based on the system Ag/AgCl//AgOTf 10 mM in EC:DMC = 1:1. Selected applications: • Corrosion studies • Spectroelectrochemical studies on inorganic metal com-plexes or organic dyes in solution (CV + UV/Vis) Item 524x - 526x - Micro reference electrodes pseudo Micro reference electrode based on metal wire (Ag or Pt); in case of type Ag/AgCl Ag wire covered with AgCl. Included: • Storage container • Connecting cable Type TSC 1600 Item No. for the respective Closed measuring cell TSC 70 TSC TSC TSC Closed Battery Surface Spectro Ag 5241 5242 5243 5244 Ag/AgCl 5271 5272 5273 5274 Pt 5261 5262 5263 5264 Selected applications • Corrosion studies • Spectroelectrochemical studies on inorganic metal com-plexes or organicdyes in solution (CV + UV/Vis) Tafel plot Autolab Microcell HC - Accessories Item 525 - Mount for Li-reference electrode 19 Elementary Li can be attached to this mount to build a Li-reference electrode; suitable for measuring cell 212 only. Amount: 5 pcs. Included: • 1 Connecting cable and 2 fittings Item 531 - Stainless steel disc electrodes* Item 532 - Nickel disc electrodes* Item 533 - Stainless steel disc electrodes gold plated* One-sided mirror-like polished disc electrodes made of stainless steel (diameter = 12 mm). Amount: 6 pcs. Item 534 - Nickel disc electrodes gold plated* One-sided mirror-like polished disc electrodes made of nickel (diameter = 12 mm). Amount: 6 pcs. Item 535 - Stainless steel disc electrodes nickel plated* One-sided mirror-like polished disc electrodes made of stainless steel (diameter = 12 mm). Amount: 6 pcs. Item 541 - Spacer set* Included: • 5 x Mylar®-foil (thickness 80 μm) • 5 x PEEK-foil (thickness 25, 50, 100 and 2 x 200 μm) Outer-diameter = 12 mm, inner-diameter = 8 mm *Only suitable for measuring cells 203, 213 and 214. Autolab Microcell HC - Accessories 20 Item 551 - Capillary-based filling set Needed for filling additional liquid solution into measuring cell through fittings while cell is closed. Included: • 1 Gas-tight Hamilton-syringe Item 552 - Capillary-based gas-inlet set Used for adding gas into measuring cell through fittings. Item 561 - Cable feed-through, with 40mm DIN flange by default The flange size depends on the requirements of the operator’s glove box. The cable feed-through contains one connecting cable Autolab Microcell HC setup/temperature contoller and 4 x BNC connecting cables. Item 571 - Faraday cage Faraday cage made of Al profile covered with acrylic glass; cable feed-through for 4 Autolab Microcell HC setups, gas inlet (p , relative = 0.5 bar). max Item 572 - Faraday cage with dew point sensor Like 571 + dew point sensor with display. Voltage rating: 85-264 VAC, 50/60 Hz Detailed technical specifications are available upon request. Autolab Microcell HC - Accessories Item 581 - Modification set item no. 101 to 102 21 Modification set needed if closed and open measuring cells should be used with the same Autolab Microcell HC setup. If an active temperature control is not necessary for the execution of your electrochemical experiments, it represents a cost-effective alternative to the Autolab Microcell HC Basic Package. Included: • Positioning unit with micrometer screw Item 582 - Passive Cell Holder Cell stand for measurements without the need for temperature control. If an active temperature control is not necessary for the execution of your electrochemical experiments, you per-form these solely at room temperature in air-conditioned rooms, it represents a cost-effective alternative to the Autolab Microcell HC Basic Package. Included: • 1 Passive cell holder • 1 Adapter box BNC - banana (item no. 442) • 2 Manuals • All required connection cables + tools No measuring cell included. Item 583 - Modification set item no. 102 to 101 Modification set needed if closed and open measuring cells should be used with the same Autolab Microcell HC setup. Included: • Connecting cable for closable cells, positioning unit Item 591 - 100 Ohm Test resistor 100 Ohm Test resistor suitable for measuring cells 203, 213 and 214. Item 599 - Transport case High-quality transport case with sufficient space for 1 x item no. 101 and 2 - 3 measuring cells. Autolab Microcell HC - Spare parts O-rings 22 Spare parts - O - rings Measuring cell Size Amount Available materials Default material TSC 70 open - - - - TSC 1600 open - - - - TSC Sw open 15 x 2.0 mm 1 FKM, EPDM, FFKM EPDM TSC 70 closed 15 x 2.0 mm 2 FKM, EPDM, FFKM EPDM TSC 1600 closed 15 x 2.0 mm 2 FKM, EPDM, FFKM EPDM TSC Sw closed 17 x 2.0 mm 2 FKM, EPDM, FFKM EPDM TSC battery 04 x 1.0 mm 4 - 8 EPDM, FFKM FFKM 10 x 1.0 mm 2 - 4 EPDM, FFKM EPDM 17 x 2.0 mm 2 EPDM, FFKM EPDM TSC surface 04 x 1.0 mm 3 FKM, EPDM, FFKM FFKM 06 x 1.5 mm 2 FKM, EPDM, FFKM FFKM 15 x 2.0 mm 1 FKM, EPDM, FFKM EPDM TSC spectro 04 x 1.0 mm 1 FKM, EPDM, FFKM FFKM 05 x 1.0 mm 2 FKM, EPDM, FFKM FFKM 06 x 1.5 mm 1 FKM, EPDM, FFKM FFKM 10 x 1.0 mm 1 FKM, EPDM, FFKM FFKM 15 x 2.0 mm 2 FKM, EPDM, FFKM FFKM Autolab Microcell HC - Spare parts TSC 70 closed Item 2111 - Thermo block with Pt crucible 23 1 Gold-plated thermo block for TSC 70 closed equipped with Pt crucible. Included: Embedded Pt00 temperature sensor. Included: • Pt100 temperature sensor equipped with Pt crucible Item 2112 PEEK housing standard 1 Housing for TSC 70 closed. Included: • 2 x O-ring 15 x 2 mm EPDM (item no. 401E) Item 2113 - Peek housing special 1 Housing for TSC 70 closed; short version allowing for low dead volume. Included: • 2 x O-ring 15 x 2 mm EPDM (item no. 401E) Important: Only compatible in combination with item no. 501 (cap with 4 glass-sealed Pt electrodes). Cap inlets cannot be used! Item 2114 - Tools, screws and O-rings Included: • 1 x Hex key 1.5 mm • 9 x Screw M2 x 5 (DIN912 A2) • 1 x Hex wrench M1.5 x 75 • 6 x O-ring 15 x 2 mm EPDM (item no. 401E) Autolab Microcell HC - Spare parts TSC 1600 closed 24 Item 2121 - Thermo block with Pt crucible 1 Gold-plated thermo block for TSC 1600 closed equipped with Pt crucible. Included • Pt100 temperature sensor equipped with Pt crucible • Embedded Pt00 temperature sensor Item 2122 - PEEK housing standard 1 Housing for TSC 1600 closed. Included: • 2 x O-ring 15 x 2 mm EPDM (item no. 401E) Item 2123 - Peek housing special 1 Housing for TSC 1600 closed; short version allowing for low dead volume. Included: • 2 x O-ring 15 x 2 mm EPDM (item no. 401E) • 1 x O-ring 14 x 2 mm EPDM Important: Cap inlets cannot be used! Item 2124 - Tools, screws and O-rings Included: • 9 x Screw M2 x 5 (DIN912 A2) • 1 x Hex key 1.5 mm • 1 x Hex wrench M1,5 x 75 • 6 x O-ring 15 x 2 mm EPDM (item no. 401E) Autolab Microcell HC - Spare parts TSC battery Item 2141 - Upper electrode for flat samples 25 1 One-sided polished stainless steel electrode (diameter 8 mm), pressed in PEEK (outer diameter 12 mm), with 2 lateral channels for O-rings. Included: • 4 x O-ring 10 x 1 mm EPDM (item no. 402E) Item 2142 - Upper electrode for contact with Li 1 Stainless steel electrode (diameter 8 mm), pressed in PEEK (outer diameter 12 mm), with 2 lateral channels for O-rings; with punching edge. Included: • 4 x O-ring 10 x 1 mm EPDM (item no. 402E) Item 2143 - Lower electrode for flat samples 1 Stainless steel electrode (diameter 8 mm), pressed in PEEK (outer diameter 12 mm), with 2 lateral channels for O-rings; with thread for thermo block at bottom side. Included: • 4 x O-ring 10 x 1 mm EPDM (item no. 402E) Item 2144 - Lower electrode for contacting Li 1 Stainless steel electrode (diameter 8 mm), pressed in PEEK (outer diameter 12 mm), with 2 lateral channels for O-rings; with punching edge and thread for thermo block at bottom side. Included: • 4 x O-ring 10 x 1 mm EPDM (item no. 402E) Item 2145 - Thermo block w/o lower electrode 1 Nickel-plated thermo block for TSC battery, with thread to fix lower electrode. Included • Embedded Pt100 temperature sensor Autolab Microcell HC - Spare parts TSC battery 26 Item 2146 - PEEK housing 1 Housing for TSC battery w/o fittings and cap. Included: • 4 x O-ring 17 x 2 mm EPDM (item no. 405E) Item 2147 - Cap with contact spring 1 Cap with contact spring for usage with TSC battery. Item 2148 - Screw for adjusting contact pressure 1 Gold-plated screw for adjusting contact pressure (in combination with item no. 21416 or 21417). Item 2149 - Fitting set and plug 1 Plug and 1 fitting for capillary-based reference electrodes and filling set, 1 fitting for usage with Li as reference electrode, all made of PEEK. Included: • 3 x O-ring 4 x 1 mm FFKM (item no. 406FF) Item 21410 - Plug 1 Plug, made of PEEK. Included: • 1 x O-ring 4 x 1 mm FFKM (item no. 406FF) Item 21411 - Capillary fitting 1 Fitting for capillary-based reference electrodes and filling set, made of PEEK. Included: • 1 x O-ring 4 x 1 mm FFKM (item no. 406FF) Autolab Microcell HC - Spare parts TSC battery Item 21412 - Li fitting 27 1 Fitting for usage of Li as reference electrode, made of PEEK. Included: • 1 x O-ring 4 x 1 mm FFKM (item no. 406FF) Item 21413 - O-ring set 16 x O-ring: 10 x 1 mm (EPDM) (item no. 402E). 02 x O-ring: 17 x 2 mm (EPDM) (item no. 405E). 03 x O-ring: 04 x 1 mm (FFKM) (item no. 406FF). Item 21414 - Tools and screws Included: • 9 x Screw M2 x 5 (DIN912 A2) • 1 x Hex key 1.5 mm • 1 x Hex key 8 mm • 1 x Rod-like tool for removing and positioning the upper electrode • 1 x Wrench for fixing lateral fittings and plug Item 21415 - 2 mm connection cable 1 Connection cable 2 mm banana plug to BNC female. Item 21416 - Pressure regulating spring 1 Gold-plated spring, standard version with spring constant = 2.3 N/mm. Gold-plated spring Item 21417 - Pressure regulating spring + 1 Gold-plated spring, strong version with spring constant = 32.6 N/mm. Gold-plated spring Autolab Microcell HC - Spare parts TSC Surface 28 Item 2151 - Thermo block 1 Gold-plated thermo block with plain surface. Included: • Embedded Pt100 temperature sensor Item 2152 - PEEK housing 1 Housing w/o fittings and cap. Included: • 2 x O-ring 15 x 2 mm EPDM (item no. 401E) • 2 x O-ring 6 x 1.5 mm FFKM (item no. 404FF) • 1 x 2 mm banana to 2 mm banana cable Item 2153 - Fitting set and plug 1 Plug, 1 fitting for capillary-based reference electrodes and filling set, 1 fitting for usage with Li as reference electrode, all made of PEEK. Included: • 3 x O-ring 4 x 1 mm FFKM (item no. 406FF) Item 2154 - Plug 1 Plug made of PEEK. Included: • 1 x O-ring 4 x 1 mm FFKM (item no. 406FF) Item 2155 - Capillary fitting 1 Fitting for capillary-based reference electrodes and filling set, made of PEEK. Included: • 1 x O-ring 4 x 1 FFKM (item no. 406FF) Autolab Microcell HC - Spare parts TSC Surface Item 2156 - Li fitting 29 1 Fitting for usage of Li as reference electrode, made of PEEK. Included: 1 x O-ring 4 x 1 FFKM (item no. 406FF) Item 2157 - Tools and screws Included: • 9 x Screw M2 x 5 (DIN912 A2) • 1 x Hex wrench M1.5 x 75 • 1 x Hex key 1.5 mm • 1 x Wrench for fixing lateral fittings and plug Autolab Microcell HC - Spare parts TSC Spectro 30 Item 2161 - Thermo block 1 Gold-plated thermo block with plain surface. Included: • Embedded Pt 100 temperature sensor Item 2162 - Pt Gauze electrode 1 Pt gauze electrode. Item 2163 - Peek housing 1 Housing consisting of 2 separate parts, w/o optical windows and cap. Included: • 2 x O-ring 10 x 1 mm FFKM (item no. 402FFKM) • 3 x O-ring 15 x 2 mm FFKM (item no. 402FF) • 3 x Screw M2 x 5 (DIN912 A2) Item Item 2164 - Optical window 1 Peek screw fitting with optical quartz window. Included: • 2 x O-ring 5 x 1 mm FFKM (item no. 407FF) Item 2165 - Col imating lens kit 2 x SMA Adaptor unit. Included: • 2 x Collimating lenses Item 2166 - Fitting for reference electrode 1 Fitting for capillary-based reference electrode or Ag-pseudo reference electrode, type TSC spectro, and filling set. Included: • 1 x O-ring 4 x 1 mm FFKM (item no. 406FF) Autolab Microcell HC - Spare parts TSC Spectro Item 2167 - Tools and screws 31 Included: • 9 x Screw M2 x 5 (DIN912 A2) • 9 x Screw M2 x 8 (DIN912 A2) • 1 x Hex wrench M1.5 x 75 • 1 x Wrench for fixing lateral fittings and plug • 1 x Hex key 3 mm www.metrohm.com Subject to change Number TBC April 2018