TECHNICAL BULLETIN 935 For the Most Demanding cGLP/GMP Laboratories The DDM 2909 Automatic Density Meter Densitometry Applications Flexible Method Management The DDM 2909 Density Meter, with high precision Peltier Factory installed density meter measurement methods allow temperature control of sample, has the features for immediate selection of the correct method to match the to meet the needs of today’s industries. most common applications. PETROLEUM • Measure API Values in accordance with ASTM D1250, ASTM D4052, ASTM D5002 and DIN 51757 • QC incoming raw materials • Research new products and additives • Withstands harsh and heavy use environments • Calibrate using petroleum standards CHEMICAL • Measure in units of Kg/m3, g/cm3, g/ mL, pounds/gallon, specific gravity, Baumé and more For unique measurement applications, create a sample method using an unlimited number of Concentration Tables, Formulas, • Determine concentrations in: %, and Polynomials to match the measurement methods used molarity, normality, mole fraction, in your laboratory. A few customized sample methods shown ppm, and more below: • Check batch consistency and ensure proper blending ratios • Baumé of Hydrochloric Acid • % HNO3 • Wetted materials compatible with the • Normality of Sulfuric Acid • Monomer Solutions most aggressive chemicals • Density of Gasses and Aerosols • Potassium Permanganate • Drug to Propellant Ratio • Hydrogen Peroxide PHARMACEUTICAL • Lead Content • Molar Solutions of EDTA • • • Capable of multiple measurements ppm Gold in Acid SG of Urine with standard deviation, min • % Toluene in Heptane • Sweeteners and max reading for true • Fat in Lubricant • Sodium Hydroxide cGLP/GMP compliance • Mole Fraction of Methanol • Complete IQ/OQ/PQ documentation Setting up your custom method on your Density Meter is • Checking of raw materials and as simple as filling out a few screens like the one below: product release • 21CFR11 Compliance; Electronic Signature and Secure Data Storage • Compliant with USP 29<841>, JP, BP and EP BEVERAGE • Measure both alcoholic and non-alcoholic beverages with easy bubble detection using VideoView™ • Direct and accurate means of °Brix determination, °Plato, Extract, % Solids • Use apparent density function for proper filling volume monitoring Rudolph Research Analytical 55 Newburgh Road, Hackettstown, NJ 07840 USA • Phone: 973-584-1558 • Fax: 973-584-5440 • E-mail: info@rudolphresearch.com • Internet: www.rudolphresearch.com The Simplicity of Touch Screen Measurement with the Flexibility of Embedded Windows® 7 Full Feature VideoView™ VideoView™ provides superior high resolution visual bubble The video clarity, magnification, and resolution mean no more detection within your samples with live on-screen video straining to see small difficult-to-detect air bubbles in your viewing. Rudolph’s industry leading 10X magnification aids in sample. Rudolph’s exclusive VideoView™ is protected under identifying bubbles if present in the sample. Patent #7,437,909. The Rudolph 2909 Density Meter offers 21CFR Part 11 • % HNO3 Instrument Level Compliance • Monomer Solutions The DDM 2909′s 21CFR Part 11 software • Potassium Permanganate module is easily enabled through the user • Hydrogen Peroxide friendly touch screen. This module gives • Molar Solutions of EDTA you full compliance with: • SG of Urine • Electronic signature • Sweeteners • Access levels • Internal write protected storage • Sodium Hydroxide • Unique passwords • Write protected documents sent directly to server Oscillating U-Tube with Viscosity Correction and Reference Oscillator The DDM 2909 Density Meter’s oscillating U-tube with full range viscosity correction and reference oscillator allows long term calibration stability and measurement at all temperatures with a single calibration. Rudolph Research Analytical 55 Newburgh Road, Hackettstown, NJ 07840 USA • Phone: 973-584-1558 • Fax: 973-584-5440 • E-mail: info@rudolphresearch.com • Internet: www.rudolphresearch.com The Simplicity of Touch Screen Measurement with the Flexibility of Embedded Windows® 7 24-May-2012 cGMP/GLP Calibration Density Meter HELP 12:05:40 v(B)3.0.0.207 [DDM2910] • Calibrate the DDM 2909 with 2 or 3 Density Calibration Adjustment Method Information Available Calibration Adjustments Traceable Standards – calibrating with Method HCl Air, Water Measurement PERFORM merely air and water appears inconsistent Mode Multiple [5] Air, Water and 3rd Point with cGMP/GLP compliance regulations. Measurement Temperature RAPID Criteria Viscosity SETTINGS • Can print out complete method Sample Specific Gravity Barometric Pressure Sample ID configuration, communication settings, HISTORY as well as calibration verification and Lot ID Normality Heated calibration adjustment data/history. Temperature (Deg C) Interface CLOSE Set 20.00 • Measured values Hydrochloric Acid Sample 20.00 OFF can be shown ST Calibration AR Ve T rification continuously as Baume Calibration Verifications List temperature stability VIDEO Water at 25C PERFORM is being reached or, at Water at 20C MENU METHOD PRINT EXPORT AIR PUMP ACCESSORIES NIST Toluene Standard the discretion of the ADD user, measured values • Unlimited number of customized will only be displayed EDIT calibration adjustments and once the final answer calibration verifications possible. is reached and DELETE completely stable. • Complete History of Calibration Adjustments and Verifications are HISTORY available to View, Print, and/or Export CLOSE • Possible to set calendar reminders as to when Calibrations are due Computer Windows Based Flexibility • 2 gigabytes of internal Compact Flash Memory . • The DDM 2909 Density Meter is network ready and data may also be saved directly to your server or to any directory desired. • Internet access is possible directly from the DDM 2909′s touch screen. • Disk Protection feature protects the operating system against malware infections in networked environments. • Windows based navigation architecture is so intuitive that most operators will never read the manual. But should you wish to reference the manual, it is stored right on the DDM 2909′s internal memory • Copy methods, transfer concentration tables, download data, etc., via the USB ports. • Three USB ports allow for quick and easy connection to a mouse, keyboard, printer, bar code scanner, or memory stick. Rudolph Research Analytical 55 Newburgh Road, Hackettstown, NJ 07840 USA • Phone: 973-584-1558 • Fax: 973-584-5440 • E-mail: info@rudolphresearch.com • Internet: www.rudolphresearch.com Full cGMP/GLP Compliance cGMP/GLP Printing Sample measurement reports are edited quickly and easily. Just import your logo to the DDM 2909 Density Meter and print your company’s customized “C of A” directly. Print your customized Certificate of Analysis including your company logo directly from the DDM 2909 touch screen Rudolph Research Analytical 55 Newburg Road Hackettstown, NJ 07840 USA Date: 26-Jan-2007 This sample was measured on DDM 2909 serial number 20212, manufactured by Rudolph Versatile Communication Capability Research Analytical, Hackettstown, NJ, USA. The DDM 2909′s standard communication package includes: Lot ID 2019 • Touch Screen User Interface Temperature: 20.0 Deg C • 3 USB ports (2 Rear, 1 Front) No Sample ID Density Sp. Gravity Normality HCL % wt ° Baume Time • 1 – Ethernet Cat 5 Port 1 8421 1.0980 1.1000 6.009 19.95 12.94 14:20:50 PM 1 8421 1.0980 1.1000 6.009 19.95 12.94 14:21:40 PM Allowing the capability to: 1 8421 1.0980 1.1000 6.009 19.95 12.94 14:22:30 PM 1 8421 1.0980 1.1000 6.009 19.95 12.94 14:23:20 PM 1 8421 1.0980 1.1000 6.009 19.95 12.94 14:24:10 PM • Connect Directly to Rudolph Service and Technical Support • Connect to any Windows® based Printer via USB or direct to the server via Windows® Print Library Counts : 5 Average : 1.0980 SD : 0.0000 • Save measurement data locally and directly to Maximum : 1.0980 Minimum : 1.0980 your Network/Server. Capable of making multiple measurements on a single sample and reporting complete statistical data and all measurement results Standard Accessories The DDM 2909 standard accessories include: • Quick Start Guide • Rinse/Sample Waste Container • Filling Nozzles • IQOQPQ Documentation • Luer Syringes • Connecting Fittings & Tubing NIST Standards Available • Manual Rudolph Research Analytical 55 Newburgh Road, Hackettstown, NJ 07840 USA • Phone: 973-584-1558 • Fax: 973-584-5440 • E-mail: info@rudolphresearch.com • Internet: www.rudolphresearch.com Automation Flexibility • Two sample loading modes; pressurized and suction; for optimizing sample transfer and measurement • Rudolph’s AutoSampler can be loaded with up to 240 samples • Customer’s unique sample bottles may be used to eliminate the need to transfer samples into special • Combine density and specific gravity measurements sized test tubes. with a polarimeter, refractometer, and colorimeter for simultaneous measurements of: • Emergency samples measured at any time without – Density/Specific Gravity stopping the AutoSampler or moving sample vials. – Refractive Index • Numerous configurations and solutions. Call us today for – Color the solution that is right for your application. – Optical Rotation/Specific Rotation • Up to three different rinse solvents available for use; fully programmable Specifications of the DDM 2909 Measurement Density: 0 to 3 g/cm3 Display: 10.4 inch diagonal TFT type LCD with Ranges: Temperature: 15 °C to 30 °C wide viewing angle, anti-glare flat panel (controlled via Peltier) touch screen, 300 nits brightness, 800 x Pressure: 0 to 10 bars 600 pixels, chemical and scratch resistant Measurement monitor, the industry’s largest and most Continuous, Single, Multiple Modes: flexible interface Measurement Communication Touch Screen User Interface Mechanical Oscillator Method Technique: Interface: 3 – USB Ports (2 Rear – 1 Front) 2 – RS232 Ports Accuracy: Density: 0.0003 g/cm3 with a single Ethernet Port for Network Connection, calibration and measurement through Keyboard, Bar Code Scanner, Mouse, multiple temperatures Network Capabilities Density: 0.0002 g/cm3 with a single Video & Video assisted, capable of Magnification: approximately 10X magnification calibration at the measurement temperature Internal Memory: 2GB Non-removable Compact Flash Temperature: 0.05 °C Operating 18.00′ (L) 11.00′ (W) 21.00′ (H) Dimensions: 46cm (L) 28cm (W) 53cm (H) Repeatability: Density: 0.0001 g/cm3 Shipping Weight: 46 lbs. (22 Kg) Temperature: 0.02°C Power Supply: 85 to 260 VAC; 48 to 62 Hz Resolution: Density: 0.0001g/cm3 Power Temperature: 0.01°C Consumption: 150-200 Watts Sample Volume: Less than 1ml Wetted Materials: Borosilicate glass, Teflon (PTFE, ECTFE) Operating System: Embedded Windows; embedded software safe from malware and viruses Rudolph Research Analytical 55 Newburgh Road, Hackettstown, NJ 07840 USA • Phone: 973-584-1558 • Fax: 973-584-5440 • E-mail: info@rudolphresearch.com • Internet: www.rudolphresearch.com 8RRA12-07 4/13