DDM 2910 DDM 2911 DDM 2911 PLUS Accuracy Density: 0.0001 g/cm3 Density: 0.00005 g/cm3 Density: 0.00001 g/cm3 Temperature: 0.05 °C Temperature: 0.03 °C Temperature: 0.01 °C TECHNICAL BULLETIN 935 Repeatability Density: 0.00005 g/cm3 Density: 0.00001 g/cm3 Density: 0.000005 g/cm3 Temperature: 0.02 °C Temperature: 0.01 °C Temperature Selectable: 0.001 °C Resolution Density: 0.0001 g/cm3 Density: 0.00001 g/cm3 Density: 0.000001 g/cm3 For High Accuracy Applications Temperature: 0.01 °C Temperature: 0.01 °C Temperature Selectable to: 0.001°C Density Ranges 0 to 3 g/cm3 Temperature Range 0 °C to 95°C (controlled via Peltier) The DDM Series of Pressure 0 to 10 bars Automatic Density Meters Video Scanning & Three magnified video assisted views of the entire cell are available, in 2x, 6x and a 10x Magnification magnifications with video scanning. Images maybe saved with results for subsequent review. Automatic Bubble Automatically warns operator of bubbles Detection Measurement Modes Continuous, Single, Multiple Measurement Technique Mechanical Oscillating U-Tube Method Minimum Sample Volume Less than 1mL Wetted Materials Borosilicate glass, Teflon PTFE ECTFE Operating Systems Windows 7® Embedded; write protected software safe from maleware and viruses Measurement Time: 30 - 60 seconds after thermal equilibration Display 10.4 inch diagonal TFT type LCD with wide viewing angle, anti-glare flat panel touch screen, 300 nits brightness, 800 x 600 pixels, chemical, scratch and spill resistant monitor, the industry’s largest and most flexible interface Communication Touch Screen User Interface, 5 – USB Ports, 2 – RS232 Ports, Ethernet Port for Network Interface Connection, Keyboard Bar Code Scanner, Mouse, Network Capabilities Remote Support Touble shooting, Diagnostics, Software Updates available via the Internet Internal Memory 8 GB Non-removable Compact Flash Operating Dimensions 18.36” (L) x 11.80” (W) x 13.90” (H) 46.61 cm (L) x 29.97 cm (W) x 35.30 cm (H) Shipping Dimensions 24.5” (L) x 17.5” (W) x 22” (H) and Weight 62cm (L) x 44cm (W) x 56cm (H) Shipping Weight 50 lbs. (23kg) Power Supply 85 to 260 VAC; 48 to 62 Hz Power Consumption 140 Watts at peak Origin of Manufacture USA and Design The Simplicity of Touch Screen Measurement with the Flexibility of Windows® 7 Full Feature VideoView™ with Automatic Scanning of Entire U-Tube Rudolph’s exclusive VideoView is protected under Patent #7,437,909 and provides superior high resolution visual bubble detection within your sample with live on-screen video viewing. Images can be saved with the sample results and may be viewed and or printed as desired. A full view of the entire U-tube is possible at 2x magnification without any obstruction. Further, the U-Tube can be scanned at 6x or 10x magnification so the user can see that the U-Tube is bubble free. The 10X magnification is also extremely helpful in detecting the cleanliness of the glass U-tube. The clarity, magnification and resolution are the very best available. • Three magnified video assisted views of the entire cell are available, in 2x, 6x and a 10x magnifications • Images maybe saved with results for subsequent review • Automatic Bubble detection is available which will flag the sample(s) with suspected bubbles Barcode Scanner USB Thumb Drive Computer Windows 7 Embedded Based Flexibility • 8 gigabytes of internal memory allows almost Browse For Folder ? X unlimited capacity for saving measurement Density Mete Select a dire r 24-May-2012 ctory to store the result HELP 12:05:40 data. All Rudolph DDM Series Density meters Export Settings are network ready and data may also be saved Density Method Information My Computer + Local Disk (C) directly to your server or to any desired directories Export Data Yes Method + HP v125w (D) HCl + densitymeter on ‘172.27.32.135’ (P:) • Internet access is possible directly from all Measurement Data Location + Mode Multiple [5] densitymeter on ‘172.27.32.163’ (Q:) Rudolph DDM Density meters touch screen. + densitymeter on ‘172.27.32.151’ (R:) Measurement + Criteria Control Panel RAPID The disk protection feature protects the + Shared Documents operating system against malware infections in Specific Gravity Sample File Naming Option User Defined networked environments Sample ID User Defined File Name Results Exp Make New Folder OK Cancel • Windows based navigation architecture is Lot ID Normality so intuitive that most operators will never File Types CSV Temperature (Deg C) Heated Interface read the manual, but should you wish to Set Delimiter Comma 20.00 Overwrite file reference the manual, it is stored right on Hydrochloric Acid Sample 20.00 Append to file OFF the Rudolph DDM’s internal memory START • Copy methods, transfer concentration tables, Baume FIELD SETTINGS AUTO EXPORT SAVE SAVE download data, etc., via the USB ports SETTINGS VIDEO on the front and back of the unit • Five USB ports allow for quick and easy connection MENU METHOD PRINT EXPORT AIR PUMP ACCESSORIES to a mouse, keyboard, printer, bar code scanner, or memory stick. Embedded Windows 7 prevents any and all viruses and malware Rudolph Research Analytical 55 Newburgh Road, Hackettstown, NJ 07840 USA • Phone: 973-584-1558 • Fax: 973-584-5440 • E-mail: info@rudolphresearch.com • Internet: www.rudolphresearch.com The Simplicity of Touch Screen Measurement with the Flexibility of Windows® 7 Oscillating U-Tube with Viscosity Correction and Reference Oscillator Rudolph DDM Density meters utilize an oscillating U-tube with full range viscosity correction and reference oscillator that allows for long term calibration stability and measurement at all temperatures with a single calibration. (Patent # 7,735,353) cGMP/GLP Calibration • Calibrate the Rudolph DDM Density Meter with 2 Density Meter 24-May-2012 HELP 12:05:40 or 3 NIST Traceable Standards – calibrating with Calibration Adjustment merely air and water appears inconsistent with Density Method Information Available Calibration Adjustments cGMP/GLP compliance regulations Method HCl Air, Water Measurement PERFORM • Can print out complete method configuration, Mode Multiple [5] Air, Water and 3rd Point communication settings, as well as calibration Measurement Temperature Criteria RAPID verification and calibration adjustment data/history Viscosity SETTINGS Calibration Verification Specific Gravity Sample Barometric Pressure Calibration Verifications List • Measured values can be shown continuously as Sample ID Water at 25C PERFORM temperature stability is being reached or, at the HISTORY Water at 20C Lot ID discretion of the user, measured values will only be Normality NIST Toluene Standard displayed once the measurment is complete Temperature (Deg C) Heated ADD Interface CLOSE • Unlimited number of customizable calibration Set 20.00 Hydrochloric Acid adjustments and calibration verifications possible Sample 20.00 EDIT OFF • Complete History of Calibration Adjustments and Verifications are available to View, Print, and/or Export START Baume DELETE • Set calendar reminders as to when Calibration VIDEO Verifications are due HISTORY MENU METHOD PRINT EXPORT AIR PUMP ACCESSORIES CLOSE Rudolph Research Analytical 55 Newburgh Road, Hackettstown, NJ 07840 USA • Phone: 973-584-1558 • Fax: 973-584-5440 • E-mail: info@rudolphresearch.com • Internet: www.rudolphresearch.com Rudolph Research Analytical 55 Newburgh Road, Hackettstown, NJ 07840 USA • Phone: 973-584-1558 • Fax: 973-584-5440 • E-mail: info@rudolphresearch.com • Internet: www.rudolphresearch.com Versatility, Traceability, Compliance and Flexibility Versatile Communication Capability The Rudolph DDM Density Meter’s standard communication package includes: • CAT 5 Ethernet Port for Network Cable Connection • 5 USB ports • 1 RS 232 ports Allowing the capability to: • Export measurement results with saved video view images to a thumb drive, store it locally on the C:\ drive, or easily send data to any external PC, LIMS, SAP, etc • Print measurement results to any local or networked printer. Most all printers are supported by Windows 7® but if required the driver may be added • Save measurement data direct to your Network/Server cGMP/GLP Printing Sample measurement reports are edited quickly and easily. Just import your logo to the Rudolph DDM Density Meter and send your company’s customized certificate of analysis to your server or local printer. Print your customized Certificate 1-40, Goryo Ohara, Nishikyo-ku, of Analysis including your Kyoto 615-8245, Japan Tel: +81-75-382-1411 company logo directly from the DDM Density Meter touch screen Date: February 19, 2014 This sample was measured on DDM 2911 PLUS serial number 20212, manufactured by Rudolph Research Analytical, Hackettstown, NJ, USA. Lot ID 2019 Temperature: 20.0 Deg C No Sample ID Density Sp. Gravity Normality HCL % wt ° Baume Time 1 8421 1.09803 1.1000 6.0092 19.95 12.94 14:20:50 PM Capable of making multiple 1 8421 1.09803 1.1000 6.0092 19.95 12.94 14:21:40 PM measurements on a single sample 1 8421 1.09803 1.1000 6.0092 19.95 12.94 14:22:30 PM 1 8421 1.09803 1.1000 6.0092 19.95 12.94 14:23:20 PM and reporting complete statistical 1 8421 1.09803 1.1000 6.0092 19.95 12.94 14:24:10 PM data and all measurement results Counts : 5 Average : 1.0980 SD : 0.0000 Maximum : 1.0980 Minimum : 1.0980 Operator : ___________________________ Rudolph Research Analytical 55 Newburgh Road, Hackettstown, NJ 07840 USA • Phone: 973-584-1558 • Fax: 973-584-5440 • E-mail: info@rudolphresearch.com • Internet: www.rudolphresearch.com Versatility, Traceability, Compliance and Flexibility NIST Traceable Calibration Standards Rudolph knows how important it is to calibrate with Traceable Standards and therefore, we include either a NIST or UKAS standard in the accessories provided with your density meter. The Rudolph DDM Density Meters includes all the accessories for immediate use which includes: • Quick Start Guide • Traceable Standard • IQOQPQ Documentation • Luer Syringes • Rinse/Sample Waste Container • User Manual • Filling Nozzles • Tools • Connecting Fittings & Tubing Full 21CFR Part 11 Instrument Level Compliance The The Rudolph DDM Density Meter’s 21CFR Part 11 software module is easily enabled through the user friendly touch screen. This module gives you full compliance with: • Electronic signature • Audit Trail • Access levels • PDF Meta Data • Internal write protected storage • Unique passwords • Write protected documents sent directly to server Flexible Method Management Customized Methods: Factory installed measurement methods allow for immediate selection of the correct method to match • Concentration D2O – Heavy Water the most common applications. • Proofing of Ethanol Sample For unique measurement applications, easily create a sample • Density of Gasses method using an unlimited number of Concentration Tables, Formulas, and Polynomials to match the measurement methods • Testing of aspartame and other artificial sweeteners used in your laboratory. • Monomer Solutions • Hydrogen Peroxide Method Management • Determination of Partial Specific Volume NAME TYPE ADD • ppm, Normality, Molarity AOAC Ethanol Factory Brix Factory COPY • % Toluene in Heptane Crude Oil Factory • Mole Fraction of Methanol Density Factory HIDE Density Continuous Factory • Purity of sample testing Density through Temperature Factory RENAME • Density of Gasses and Aerosols Density VC Factory VIEW Factory QC Testing Factory • Potassium Permanganate Fuel Oil Factory RESULTS • Sweeteners Lubricants Factory OIML Ethanol Factory • Ultracentrifugation applications METHOD CONFIGURATION • SG of Urine CLOSE • Sodium Hydroxide Rudolph Research Analytical 55 Newburgh Road, Hackettstown, NJ 07840 USA • Phone: 973-584-1558 • Fax: 973-584-5440 • E-mail: info@rudolphresearch.com • Internet: www.rudolphresearch.com Automation Solutions Automate your Laboratory with a Rudolph AutoFlex R837 Automation System The DDM Series of density meters can be combined with various Rudolph Automation Systems and Sample Handling Accessories. Available are Peristaltic Pumping, Heated Sampler, the ECS (Easy Clean System), and the Rudolph R837 AutoFlex Sampler. The Rudolph Research R837 AutoFlex is perfect for high throughput laboratories looking to increase productivity The R837 AutoFlex Sampler Facilitates: • Customizable bottle size, Test Tube size, Boston Rounds:1oz, ½ oz, virtually any size • Customizable Rack configurations: heated and unheated on the same carousel • Automated sample introduction • Flexible Method Selection: Suction mode, Pressure mode, Rinse and Dry Duration • Programmable cleaning and drying • Automatic solvent and waste level detection • System Configuration minimal sample volume: 1.5 mL • A heated interface is available • Fast throughput, 2-5 min complete cycle time • Automation saves operator time and increases your lab’s efficiency • An urgent-sample interruption can be made at any time Operation is completely automatic. The sample is measured and the data recorded. Depending on how the system is configured the data may also be printed, saved as an Excel file or transferred to a LIMS system. Flow through Configuration with ECS: Density Meter, Refractometer Optics Module and a Rudolph (ECS) Easy Clean sampling System Description This configuration is the most versatile. The user loads the sample in a similar way to the peristaltic pump system but after the measurement; the instrument disposes of the sample to waste, rinses with two solvents and then dries with air from the built in pump. Who should consider this system? • Users who want the ease of automated loading and cleaning • Users with samples that have too high a viscosity to be pumped with a peristaltic pump • Users who have a significant amount of samples but not enough to require full automation Refractometer Measurement Module Syringe Pump Rinse & and Air Pump Solvent Metal Sipper nose 50ml of Sample Waste Container Peristalic With Over Fill Warning Pump Option Rudolph Research Analytical 55 Newburgh Road, Hackettstown, NJ 07840 USA • Phone: 973-584-1558 • Fax: 973-584-5440 • E-mail: info@rudolphresearch.com • Internet: www.rudolphresearch.com Rudolph Research Analytical 55 Newburgh Road, Hackettstown, NJ 07840 USA • Phone: 973-584-1558 • Fax: 973-584-5440 • E-mail: info@rudolphresearch.com • Internet: www.rudolphresearch.com Densitometry The Rudolph DDM series of density meters, with high precision Peltier temperature control of sample, has the features to meet the needs of today’s industrial applications. BEVERAGES, SPIRITS, WINE PETROLEUM, CHEMICAL • The US Alcohol and Tobacco Tax and • Measure API, Density and Specific Trade Bureau (TTB) requires 0.02% Gravity values in accordance with ASTM D1250, ASTM D4052, ASTM Ethanol accuracy for testing of % D4806, ASTM D5002, ASTM D5931, Ethanol in wine, beer, and spirits for ISO 12185 and DIN 51757 the purposes of taxation and labeling • Measure in units of Kg/m3, g/cm3, • The DDM2911 Plus offers 0.01% g/mL, pounds/gallon, specific gravity, accuracy for Ethanol testing Baumé and more • Direct and accurate means of • Check batch consistency and ensure °Brix determination, °Plato, proper blending ratios °Balling, Proof, % Solids • Withstands harsh environments and aggressive chemicals • Calibrate using petroleum standards FOOD, FLAVOR, FRAGRANCE PHARMACEUTICAL • Measure Density, Specific Gravity • Capable of 2,3,4 or more multiple • Checking of raw materials and product measurements with standard release deviation, mean, min and max reading • Check batch consistency and ensure for true cGLP/GMP compliance proper blending ratios • Complete IQ/OQ/PQ documentation. • May add refractive index, color • Checking of raw materials and product and optical rotation to the density release measurement • 21CFR11 Compliance; Electronic Signature and Secure Data Storage. • Compliant with USP <8417>, JP, BP and EP Alcohol Proof Testing DDM 2911 PLUS Density Meter is a Rudolph Research’s TTB Approved Instrument for Alcohol Proof Testing. The capability you need to easily test your spirits production and comply with TTB Requirements: The DDM 2911 PLUS has built-in precision Electronic temperature control ensuring accurate and reproducible results. A Windows 7 embedded OS allows the operator to save calibration and measurement data right to ExcelTM. • With 0.00001 g/cm3 accuracy the DDM 2911 PLUS is an excellent choice for the Alcohol Beverage industry to measure alcohol concentration to determine alcohol Proof • Easy to Use • Easy to Validate • Windows 7 Embedded OS integrates easily with you current systems • Precision built-in electronic Temperature Control • Easily combined with Rudolph’s R837 Automation System • 3 Year Warranty – 20 Year service Guarantee 0.01% Alcohol Determination adding Precision to the Art of Craft Distilling Rudolph Research Analytical 55 Newburgh Road, Hackettstown, NJ 07840 USA • Phone: 973-584-1558 • Fax: 973-584-5440 • E-mail: info@rudolphresearch.com • Internet: www.rudolphresearch.com Specifications DDM 2910 DDM 2911 DDM 2911 PLUS Accuracy Density: 0.0001 g/cm3 Density: 0.00005 g/cm3 Density: 0.00001 g/cm3 Temperature: 0.05 °C Temperature: 0.03 °C Temperature: 0.01 °C Repeatability Density: 0.00005 g/cm3 Density: 0.00001 g/cm3 Density: 0.000005 g/cm3 Temperature: 0.02 °C Temperature: 0.01 °C Temperature Selectable: 0.001 °C Resolution Density: 0.0001 g/cm3 Density: 0.00001 g/cm3 Density: 0.000001 g/cm3 Temperature: 0.01 °C Temperature: 0.01 °C Temperature Selectable to: 0.001°C Density Ranges 0 to 3 g/cm3 Temperature Range 0 °C to 95°C (controlled via Peltier) Pressure 0 to 10 bars Video Scanning & Three magnified video assisted views of the entire cell are available, in 2x, 6x and a 10x Magnification magnifications with video scanning. Images maybe saved with results for subsequent review. Automatic Bubble Automatically warns operator of bubbles Detection Measurement Modes Continuous, Single, Multiple Measurement Technique Mechanical Oscillating U-Tube Method Minimum Sample Volume Less than 1mL Wetted Materials Borosilicate glass, Teflon PTFE ECTFE Operating Systems Windows 7® Embedded; write protected software safe from maleware and viruses Measurement Time: 30 - 60 seconds after thermal equilibration Display 10.4 inch diagonal TFT type LCD with wide viewing angle, anti-glare flat panel touch screen, 300 nits brightness, 800 x 600 pixels, chemical, scratch and spill resistant monitor, the industry’s largest and most flexible interface Communication Touch Screen User Interface, 5 – USB Ports, 2 – RS232 Ports, Ethernet Port for Network Interface Connection, Keyboard Bar Code Scanner, Mouse, Network Capabilities Remote Support Touble shooting, Diagnostics, Software Updates available via the Internet Internal Memory 8 GB Non-removable Compact Flash Operating Dimensions 18.36” (L) x 11.80” (W) x 13.90” (H) 46.61 cm (L) x 29.97 cm (W) x 35.30 cm (H) Shipping Dimensions 24.5” (L) x 17.5” (W) x 22” (H) and Weight 62cm (L) x 44cm (W) x 56cm (H) Shipping Weight 50 lbs. (23kg) Power Supply 85 to 260 VAC; 48 to 62 Hz Power Consumption 140 Watts at peak Origin of Manufacture USA and Design Rudolph Research Analytical 55 Newburgh Road, Hackettstown, NJ 07840 USA • Phone: 973-584-1558 • Fax: 973-584-5440 • E-mail: info@rudolphresearch.com • Internet: www.rudolphresearch.com 12RRA935 1/15