MILESTONE H E L P I N G C H E M I S T S FAST & REPRODUCIBLE CARBON BLACK DETERMINATION IN OLEFIN PLASTIC PYRO HIGH SAMPLE THROUGHPUT SUPERIOR EASE OF USE HIGH PRODUCTIVITY SELF-CLOSING CRUCIBLES GREAT REPRODUCIBILITY EQUIVALENT TO ASTM D1603 M A X I M I Z E EASE OF USE IN POLYMER QC LABS The addition of carbon black to an elastomer can have nitrogen. The vacuum generated during the release a positive effect upon its mechanical, electrical and of combustion fumes ensures perfect sealing and an physical properties. Therefore, QC and process labs inert athmosphere the quartz crucibles, allowing for need to determine the exact concentration of carbon complete determination of the carbon black. The self-to ensure product quality and monitor production closing quartz crucibles and microwave heating allow costs. A rapid determination of the carbon black for carbon black determination in only a few minutes, content allows quick feedback to production and for obtaining superior data reliability and reproducibility. adjustment when required. A standard approach to this analysis is ASTM D1603, which provides gravimetrical determination of carbon black content following a lengthy pyrolysis step under nitrogen. Milestone has developed a dedicated configuration to overcome the limitations of the traditional approach, such as the use of nitrogen, and to expedite the ashing process. The use of Milestone’s PYRO muffle furnace (High Sample Throughput configuration) along with self-closing quartz crucibles and dedicated rack (20 positions) ensures fast determination and high reproducibility compared with the reference method, thus avoiding the use of Self-closing quartz crucibles with 20 position rack Polyethylene Polypropylene Carbon Black RSD Carbon Black RSD (%) (n=5) (%) (%) (n=5) (%) PYRO 40.1 1.18 18.3 2.03 (High Sample Throughput) ASTM D1603 40.1 1.06 18.4 1.85 Typical results CAT387EN-001 • 2018-11 MILESTONE MILESTONE Srl - Via Fatebenefratelli, 1/5 - 24010 Sorisole (BG) - Italy MILESTONE GENERAL K.K. - KSP, 3-2-1, Sakado - Takatsu-Ku, Tel: +39 035 573857 - Fax: +39 035 575498 Kawasaki 213-0012 - Japan - Tel: +81 (0)44 850 3811 - Fax: +81 (0)44 819 3036 www.milestonesrl.com - email: analytical@milestonesrl.com www.milestone-general.com - email: info@milestone-general.com MILESTONE INC. - 25 Controls Drive - Shelton, CT 06484 - USA MLS GmbH - Auenweg 37 D-88299 Leutkirch im Allgau - Germany Tel: (203) 925-4240 - Toll-free: (866) 995-5100 - Fax: (203) 925-4241 Tel: +49 (0)7561 9818-0 - Fax: +49 (0)7561 9818-12 H E L P I N G C H E M I S T S www.milestonesci.com - email: mwave@milestonesci.com www.mls-mikrowellen.de - email: mws@mls-mikrowellen.de