TECHNICAL BULLETIN 928 For the Most Demanding High Accuracy Applications The Autopol® V PLUS and Autopol® VI The brand of polarimeter used in more labs than any other.* *Emmes Survey The most stringent pharmaceutical requirements Autopol VI or Built in Three Rotation Acid Resistant Autopol® V PLUS NIST Calibration Standard Cell Chamber and Temperature Probe Acid Resistant Ceramic Cell Patented TempTrolTM Heating and Cooling System 6,717,655 Easy Access USB for a Tiltable Screen for Autopol® V PLUS and VI Wireless Mouse or Keyboard all Operator Heights data connections on back of unit Unmatched Accuracy: ± 0.0003° Arc NIST Traceable Measurement Calibration Accessories Included With Instrument Purchase For Racemic Solutions and very low concentration samples, the Autopol® VI provides unmatched 4th decimal optical rotation accuracy of ±0.0003°Arc over ±1°Arc. Instrument performance for readings between -1 and 1° Arc is: Resolution ±0.0001, Reproducibility ±0.0002, and Accuracy ±0.0003. The Industry Standard Polarimeter The Autopol® V PLUS and Autopol® VI have the validation tools and features to satisfy today’s global pharmaceutical companies, including: instrument level 21CFR Part 11 compliance, NIST traceable calibration standards and a global list of installations. Rudolph Research has thousands of satisfied customers who praise the Autopol® V PLUS and Autopol® VI quality, accuracy and reproducibility. Autopol® V PLUS and Autopol VI Standard Features and Accessories • TempTrol™ – Electronic cooling & heating from 15°- \40°C • Six Standard Wavelengths: 365nm, 405nm, 436nm, 546nm, 589nm and 633nm • 21CFR11 Compliance: Embedded or by a separate PC • Domestic 3-year warranty and 20-year support guarantee • International warranty varies by country • Standard Accessories: TempTrol™ NIST Traceable Quartz Standard (3 rotation), TempTrol™ 100mm Polarimeter Cell, TempTrol™ Temperature Validation Cell, Thermoprobe, and Built-In Sample Measurement Probe 3 Rotation TempTrol™ NIST Traceable Quartz Calibration Standards For Hands Free Internal Optical Rotation Measurement Validation Rudolph Research Analytical 55 Newburgh Road, Hackettstown, NJ 07840 USA • Phone: 973-584-1558 • Fax: 973-584-5440 • E-mail: info@rudolphresearch.com • Internet: www.rudolphresearch.com The Autopol® V PLUS and Autopol® VI Use Rudolph’s Exclusive TempTrol™ Electronic Temperature Control System The USP <781> requires optical rotation measurements at 25°C ± .5°C (unless another temperature is specified). The (EP)European Pharmacopoeia requires optical rotation measurements made at 20° ± .5°C (unless another temperature is specified). Whatever your temperature control needs are, the Autopol® VI and the Autopol® V PLUS’ exclusive TempTrol™ System (Patent No. 6,717,665) makes your measurement in a few minutes without a water bath or any type of water circulation. The TempTrol™ System allows push-button temperature control of your 100mm cell, 200mm cell or Quartz Plate. Set the temperature, push “measure” and walk away. The Autopol® will heat or cool to a predefined temperature and then provide you with the result all in one easy step. Patented TempTrol™ Technology Eliminates the Need for a Water Bath. Here is How the TempTrol™ System Works: Temperature Measurement Port Methods For improved temperature performance or when working Setup > Methods > Edit > Temperature with acids (HCl) use the measurement port in the body of the cell. This also allows the inlet and outlet ports to be capped to avoid evaporation, fumes and spillage. Temp Correction Off Temp Control Status ON Set Temp 25 °C Temperature Stability +/- 0.20 Stability Time 5 Sec Cancel Save NEDOX® Coated Temperature measurement probe Temperature is selected via touch screen. Temperature Place the TempTrol™ cell in your TempTrol™ equipped selection of 25°C shown above. Autopol® sample chamber to measure to within ±0.2°C of the TempTrol™ cell with mating heating & cooling transfer USP, EP, JP or BP specified temperature (normally 20°C or surface manufactured with acid resistance materials: 25°C ±0.5°C). NEDOX™ and Peek™ below. To Validate Temperature Performance Rudolph provides a temperature validation cell with every TempTrol™ active surface with NEDOX® coating TempTrol™ system. The temperature validation cell along with an optional NIST traceable Thermo Probe is designed to validate the temperature control performance of the polarimeter and cell to ±0.2°C. Acid Resistant Ceramic External Temperature Probe Quartz wetted inner sleeve TempTrol™ NEDOX™ passive surface mates to active surface Connect to PC or Polarimeter TempTrolTM Measurment Probe Water Port NIST Traceable extended probe for Temperature Validation and Calibration TempTrolTM Measurement Probe Port Temperature Validation Cell Rudolph Research Analytical 55 Newburgh Road, Hackettstown, NJ 07840 USA • Phone: 973-584-1558 • Fax: 973-584-5440 • E-mail: info@rudolphresearch.com • Internet: www.rudolphresearch.com Automatic Measurement Validation The only self contained and automatically loaded quartz control plates. • Calibrate your Rudolph Autopol® V PLUS and Autopol® VI Polarimeter right from the user friendly touch screen. • The Quartz Control plates stored in the instrument are automatically positioned and the calibration is performed for you. Results are recorded and you are finished. Calibration results can be stored on the local hard drive or printed for future reference. • Rudolph’s 3 rotation Quartz Standard is Traceable to NIST and certified by an internationally recognized accreditation body (NVLAP). • Labs must use multiple rotations to comply with FDA rulings – a Single Rotation Quartz Control Plate has been ruled non-compliant by the FDA. • Rudolph strongly encourages Calibration with 3 rotational values to comply with the latest FDA rulings. Your history of calibration is stored right in the instrument. 2 Quartz Plates are stored within the instrument, ready for automatic calibration. Rudolph is the only Polarimeter manufacturer in the world producing certified 3 rotation Quartz Calibration Standards accredited by NVLAP and traceable to NIST, with an accuracy of ± 0.002 degrees Optical Rotation. Negative Optical Rotation Positive Optical Rotation at 589nm = -10.7290 at 589nm = 11.5130 Combined Optical Rotation at 589nm = +0.7840 Each Quartz plate is positioned for calibration by the instrument right from the touch screen. Rudolph strongly encourages Quartz Calibration Standards Calibration is thus fully automated and requires with 3 rotational values above, below and near the sample no handling of the Quartz Control Plate. under test to comply with FDA rulings related to “Sample Bracketing” and EP’s most recent calibration guidelines on linearity. Each Quartz Standard is certified by an accredited independent body (NVLAP ) and Traceable to NIST. Rudolph Research Analytical 55 Newburgh Road, Hackettstown, NJ 07840 USA • Phone: 973-584-1558 • Fax: 973-584-5440 • E-mail: info@rudolphresearch.com • Internet: www.rudolphresearch.com Accredited to NVLAP and Traceable to NIST Optical Rotation Traceability External Temperature Probe Traceability 2018-04-01 through 2019-03-31 Ceramic Quartz Cells Luer Material is PTFE Glass window Lure PTFE Caps Temperature can be replaced Fill Port Probe Port Wetted internal parts Built – in cell apertures are ceramic quartz that are smaller than the internal cell diameter, to improve performance TempTrol™ NEDOX™ passive Turn Outer Thumb Screw surface mates to active surface to Tighten Cell in Place • Rudolph supplies Ceramic Quartz Cells as standard on • Rudolph Polarimeter cells are easy to handle, lightweight, Autopol V, V PLUS and VI polarimeters easy to fill and easy to clean. Cell ends are removable for • Cells are resistant to 6 Molar HCL – Ceramic Quartz Cells thorough cleaning. are impervious to acids and transfer heat quickly and • Rudolph Cells are light and have a large thermal transfer evenly. surface so they come to temperature quickly and • Rudolph’s exclusive, patented TempTrolTM cells use an acid evenly across the cell. resistant NEDOXTM coated transfer surface to mate with the • Cell apertures are smaller than the internal NEDOXTM coated TempTrolTM active heating and cooling bore diameter, therefore, small air bubbles do not impact transfer surface. sample measurement. Lifetime Warranty on Cells Only Rudolph provides a Lifetime Guarantee on its Ceramic Quartz Polarimeter cells covering breakage and damage caused by acids*. *According to all available marketing resources at time of printing. The Rudolph AutoFillTM Filling a Polarimeter Cell has never been easier. Rudolph Research Analytical developed AutoFillTM, Patent No. 10,101,353, a simple and easy way to allow fast and reliable polarimeter cell loading. Polarimeter sample cells are filled without bubbles, using Rudolph propriatary BubbleInspectTM technology, sample vapors are contained, and cleaning and drying is automated. Manual cell handling, cleaning and loading is eliminated. The AutoFillTM (Patent No. 10,101,353) is available as an option with BubbleInspectTM on the Autopol V Plus and Autopol VI Polarimeters. Waste Receptacle Solvent Alcohol Solvent Acetone AutoFillTM Lid Closed AutoFillTM option includes Sample BubbleInspectTM Technology Engineered for perfect fills every time. Operation is as simple as opening the AutoFillTM lid , pouring in your AutoFillTM Lid Open sample, closing the lid and pressing start. The sample will be advanced into the Polarimeter cell and stopped once full. The cell is now loaded and the measurement will automatically begin after BubbleInspectTM approves the measurement. When the measurement is complete the operator is prompted to open the AutoFillTM chamber and add a solvent. The AutoFillTM lid is closed and the solution is flushed through the cell to waste. Air drying will automatically begin and end. Open You are now ready for your next measurement. AutoFillTM reduces sample loading and cleaning time • No need to inject samples with syringes. Samples are easily poured in the AutoFillTM sample well. Closed • Eliminate contact with acids and bases. • Air dry is run for the correct amount of time to fully dry the cell. • Cleaning is made effortless. AutoFillTM Well • A perfect cell load is guaranteed every time with Rudolph’s exclusive Optical Rotation Homogeneity Inspection Solution. If Acids and Open Samples are Allowed in the Work Area • Sample is easily poured into the large AutoFillTM well. • All wetted parts are made to stand up against the most aggressive samples including 6 Molar HCl • All Materials are Teflon, Peek, and Kalrez®. • You may choose to clean with a single solvent or a combination of solvents. AutoFillTM (Patent No. 10,101,353) Rudolph Research Analytical 55 Newburgh Road, Hackettstown, NJ 07840 USA • Phone: 973-584-1558 • Fax: 973-584-5440 • E-mail: info@rudolphresearch.com • Internet: www.rudolphresearch.com The Rudolph FillStationTM Fill Rudolph Polarimeter Cells reliably outside of the instrument Many users prefer to load cells with samples outside of the Polarimeter. When this fits Rudolph Research Analytical developed AutoFillTM, Patent No. 10,101,353, a simple and easy way to allow with your work flow, Rudolph has engineered a tool to assist you, the Rudolph fast and reliable polarimeter cell loading. Polarimeter sample cells are filled without bubbles, using Rudolph Polarimeter FillStationTM. Designed to sit on your laboratory bench or under your fume propriatary BubbleInspectTM technology, sample vapors are contained, and cleaning and drying is automated. hood and assist you in loading your Rudolph Polarimeter cell easily and reliably, the Manual cell handling, cleaning and loading is eliminated. FillStationTM holds the cell at the right angle so you always fill the cell from bottom to top. Using a syringe, you inject the sample until it begins to appear at the top port. The AutoFillTM (Patent No. 10,101,353) is available as an option with Once filled, the monitoring light will become bright and you know you have a full cell BubbleInspectTM on the Autopol V Plus and Autopol VI Polarimeters. free of air bubbles that is ready for a measurement. Cap the Top Cell Port, remove the syringe, cap the Lower Port and go! Luer Screw Cap Top Outlet Cell Port Polarimeter Monitoring Light Temperature Probe Port FillStationTM Patent No. 9,677,995 On switch with 5 minute auto off Advantages of using the Rudolph FillStationTM • The cell is held at the right angle and filled from the bottom just the way Rudolph cells were designed to be filled. Perfect every time. • Filling from the bottom to top moves any air with the potential to cause a bubble up and out of the cell. • Once you see the monitoring light go to bright there is no question that the cell is properly filled. • Verification of air free sample loading for even inexperienced operators. • Helps eliminate contact with acids, bases, or any sample the user does not want to come in contact with. • Less experienced operators can learn to reliably fill cells with minimal training. The FillStationTM (Patent No. 9,677,995) is included standard with all Rudolph Autopol V, Autopol V PLUS, and VI Polarimeters. Today’s laboratories and cGMP procedures demand that noxious fumes, strong acids and other caustic materials are filled in a designated safe area where a fume hood is used and there is minimal operator exposure. Instruments are now located in clean areas or a laboratory separate from the wet area. Rudolph addresses these concerns with its FillStationTM so that cells can be easily filled and capped inside the safe wet area. Rudolph Research Analytical 55 Newburgh Road, Hackettstown, NJ 07840 USA • Phone: 973-584-1558 • Fax: 973-584-5440 • E-mail: info@rudolphresearch.com • Internet: www.rudolphresearch.com How to use the FillStationTM For users who prefer not to hold the cell while working with highly acidic or basic samples, the Rudolph Cell FillStationTM is simple and easy to use, just follow the steps below: By design, the FillStationTM will hold Place a 2.5mm or 5.0mm bore Turn the FillStationTM light on. The light the cell at a suitable angle. Polarimeter cell into the Rudolph will turn off automatically after a few FillStationTM. minutes. Please Note: Filling a Rudolph Polarimeter cell is easy and you can be assured of an air bubble free sample cell. It is important to note that when using highly acidic or basic solutions samples the cell should not be filled in the Polarimeter, doing so may allow spillage into the instrument which over time may damage the instrument. Make sure the cell is always clean and The FillStationTM creates a light image dry. Use compressed air and acetone for The Rudolph Polarimeter Cell that will go from darker to a bright this process. Fill the cell from the lower FillStationTM accessory is white circle when the cell is filled and available for all Rudolph Autopol inlet port with a Luer Syringe only. air-bubble free. A bubble free cell shows Polarimeters and included free of As the cell becomes filled and sample an illuminated white circle as shown on charge with Autopol V, Autopol V begins to appear at the upper inlet, cap the right. PLUS, and Autopol VI off the upper, then lower inlet port. Your Polarimeter Models. cell is now filled and air bubble free. Reading Your FillStationTM Empty Cell Cell Being Filled Air Bubbles detected Cell filled and free of during filling process air bubbles* How to fill cells manually Designed for syringe loading Rudolph Research Polarimeter Sample Cells are designed to be easily filled Luer Screw Cap and cleaned with a Luer syringe. When held at the correct angle and filled using the lower inlet port, the Sample will appear here The sample is injected cell is filled with almost no possibility of leaving an air bubble in the in upper outlet port. with a Luer Syringe into the lower inlet cell. Filling from the lower inlet port forces any air bubbles up and out port as seen here. of the upper outlet port. Rudolph cells are unlike other manufacturers cells as they are uniquely designed to keep small air bubbles out of the light path. Filling the cell is as simple as holding the cell at a slight upward angle and filling from the bottom inlet using a Luer Syringe. When the sample appears near the top outlet port, simply place the Luer cap on the upper port and then lower port. Your cell is now filled, capped and air bubble free. Cells must 20° to 30° Angle be clean and dry to ensure proper filling with minimum sample. Full 21CFR Part 11 Compliance Full 21CFR Part 11 Instrument Level Compliance The Autopol® V PLUS and VI’s 21CFR Part 11 software module is easily enabled through the user friendly touch screen. This module gives you full compliance with: • Electronic signature • Unique passwords • Access levels • Write protected documents sent directly to server • Internal write protected storage • Audit trail 21CFR11 mode is enabled via the Set 21CFR11 Add/Edit Users allows the creation of new 21CFR11 button. After clicking the Enable 21CFR11 button, users, the ability to edit an existing user, and the abil-the user must also select to either Enable Operator, ity to lock and unlock accounts. Enable Review or both. Rudolph Research Analytical 55 Newburgh Road, Hackettstown, NJ 07840 USA • Phone: 973-584-1558 • Fax: 973-584-5440 • E-mail: info@rudolphresearch.com • Internet: www.rudolphresearch.com Full 21CFR Part 11 Compliance Groups are used to determine the access permissions of the 21CFR11 users. When a group is added or edited, the administrator decides what menus the group will have access to in the Setup menu and sub-menus, and the 21CFR11 Administration Options menu and sub-menus. Password Settings control the password policy used by the Autopol to authenticate users and whether the screen lock function is active and how long it takes for the screen lock to turn on. Rudolph Research Analytical 55 Newburgh Road, Hackettstown, NJ 07840 USA • Phone: 973-584-1558 • Fax: 973-584-5440 • E-mail: info@rudolphresearch.com • Internet: www.rudolphresearch.com Full 21CFR Part 11 Compliance Terminology allows the Administrator to custom- ize the language of the Accept/Reject language that appears in the measurement report reviewed by a reviewer. Print your customized Certificate of Analysis including your company logo directly from the Autopol VI® touch screen The Format Printing/Output menu lets the user control what information will be contained in the report, if the report will contain a logo image, the page orientation and margin settings and if the user will be prompted for a lot identifier and sample identifier when the measurements are being performed. Rudolph Research Analytical 55 Newburgh Road, Hackettstown, NJ 07840 USA • Phone: 973-584-1558 • Fax: 973-584-5440 • E-mail: info@rudolphresearch.com • Internet: www.rudolphresearch.com The AUTOPOL® VI by Rudolph – Simply the Best ± 0.0003 Unmatched Accuracy Offered by NO OTHER BRAND All the validation tools and standard accessories required by the FDA are included 10 - 200mm Cell Length Compliant Chamber Built In Electronic Temperature HCl Resistant Control Range 10° - 35°C ± 0.5 ° C Measurement Cell Rudolph Exclusive Features Flexible Method Management Intuitive Windows® Based Interface Install your own Test Methods for immediate selection of the correct method to match your most common tests. • 32 gigabytes of internal memory allow almost unlimited capacity for saving measurement data. The Autopol® V PLUS and Autopol® VI are network ready and data may also be saved directly to your server or to any directory desired. • Internet access is possible directly from the Autopol® V PLUS and Autopol® VI’s touch screens. This feature allows real time contact with Rudolph Research Analytical’s Service and Technical Support Team who can access your instrument remotely to assist in Window navigation, method setup and trouble shooting. • Windows based navigation architecture is so intuitive that most operators will never read the manual. But should you wish to reference the manual, it is stored right on the Autopol® V PLUS and Autopol® VI’s internal memory. • Four USB ports allow quick and easy connection to a mouse, keyboard, printer, bar code scanner, or memory stick. One USB port is located on the front of the unit (shown below) and two USB ports are located on the back of the unit (shown below). Browse For Folder ? X Export Settings Select a directory to store the result Export Data Yes My Computer Data Location + Local Disk (C) + HP v125w (D) + densitymeter on ‘172.27.32.135’ (P: Polarimeter ) + densitymeter on ‘172.27.32.163’ (Q: Polarimeter ) + densitymeter on ‘172.27.32.151’ (R:) Polarimeter File Naming Option User Defined + Control Panel + Shared Documents User Defined File Name Results Exp File Types CSV Make New Folder OK Cancel Delimiter Comma Overwrite file Append to file Rudolph Research Analytical 55 Newburgh Road, Hackettstown, NJ 07840 USA • Phone: 973-584-1558 • Fax: 973-584-5440 • E-mail: info@rudolphresearch.com • Int FIELD SETTINGS AUTO EXPORT SAVE ernet: www.rudolphresearch.com SAVE SETTINGS Accessories Included With Autopol V PLUS and VI Only Rudolph Provides: 2 Lamps Lifetime Guarantee, Included NVLAP Accreditation TempTrolTM Ceramic Quartz 2,000 hours 3 Rotation TempTrolTM , measurement cell each. NIST Traceable Quartz Calibration Standard. NIST Traceable Digital Temperature Probe The Rudolph FillStationTM Patent No. 9,677,995 Temperature Validation Cell The AUTOPOL® V PLUS and AUTOPOL® VI Advantage • 6 Molar HCl acid resistance: NEDOXTM coating on the chamber, temperature transfer surface, cell surface, and temperature probe slot . • To meet the FDA’s latest position on measurement bracketing, the Autopol® V PLUS and VI comes with two NIST traceable quartz plates with three rotations: +0.998° Arc, +10.998° Arc, -10.000° Arc. Each Quartz Plate comes with a NIST Traceable Certificate and NVLAP Accreditation document. • Measurement validation is completely automated. 2 Quartz Control Plates are stored right in the instrument for a 3 rotation validation, all accomplished right from the touch screen and held in the internal QCP history database. • Temperature validation cell to ensure complience USP/EP 25°C ± 0.5°C and 20°C ± 0.5°C • Windows based navigation architecture is so intuitive that most operators will never read the manual. But should you wish to reference the manual, it is stored right on the Autopol® V PLUS and VI internal hard drive. • Rudolph’s Exclusive FillStationTM (Patent No. 9,677,995 ) is a standard accessory. • Three USB ports allow quick and easy connection to a mouse, keyboard, printer, bar code scanner, or memory stick. One USB port is located on the front of the unit (shown above) and two USB ports are located on the back of the unit (shown below). • Ethernet Port for Network Cable Connection. • Internet access allowing connection to Rudolph’s service department for remote testing and diagnostics . • Connect to any Windows® based printer via USB or direct to the server via Windows® Print Library. • Save measurement data direct to your Network/Server- LIMS or SAP (No PC or special software needed ). • Windows embedded software cannot be written to, thus virus proof. • Only Rudolph provides a lifetime guarantee on breakage and HCl resistance on its ceramic quartz sample cells. • Only Rudolph commits to servicing your instrument for 20 years or more. • Most of the polarimeters Rudolph has manufactured in the past 10, 20 and 30 years are still being used in labs today. • Rudolph sells more polarimeters than the next two manufacturers combined. Rudolph Research Analytical 55 Newburgh Road, Hackettstown, NJ 07840 USA • Phone: 973-584-1558 • Fax: 973-584-5440 • E-mail: info@rudolphresearch.com • Internet: www.rudolphresearch.com Supporting over 8,000 Instruments in over 80 Countries Just listen to our customers “We have the AUTOPOL V from Rudolph Research Analytical (RRA)... I have used numerous polarimeters and this is by far the best. We have had it for 1-1/2 years and have had zero problems, the original lamp is still in the instrument. I recommend it over other instruments. RRA installed, trained and performed the IQOQ... It is one piece of equipment that you never worry about.” Alan Davis – Rockwell Medical Technologies Rudolph Research Analytical 55 Newburgh Road, Hackettstown, NJ 07840 USA • Phone: 973-584-1558 • Fax: 973-584-5440 • E-mail: info@rudolphresearch.com • Internet: www.rudolphresearch.com Rudolph Research Analytical 55 Newburgh Road, Hackettstown, NJ 07840 USA • Phone: 973-584-1558 • Fax: 973-584-5440 • E-mail: info@rudolphresearch.com • Internet: www.rudolphresearch.com Rudolph Research Analytical Service Guarantee The Rudolph Service Pledge: The The R Rudolph Service Pledge: e Rudolph Service Pledge: ce Pledge Earning your loyalty everyday E , through our commitment to exceptional service and attentive customer focu Earning your loyalty everyday, through our commitment to arning your loyalty everyday, through our comm Earning your loyalty everyday ryday, through our itm to excepti o exc o s . Integrity, Quality, and Innovation with a Global Reach. Integrity, Quality, and Innovation ntegrity, Qua nd In Integrity, Quality, and Innovation ty, and Innovat with w a with th a Globa G Gl Rudolph Research Analytical manufactures automatic Density Meters, Refractometers, Polarimeters, Saccharimeters and Rudolph Research An anufact ytical manufactures auto Density Rudolph Research Analytical manufactures automatic D Density M Mee ers, tter R Automation Solutions for a wide variety of industries. W ation Solutions for a wide variety of industries. Automation Solutions variety r a wide variety of indus ith over 8,000 laboratory instruments installed in demanding W th over Wit ith h ov over 8 00 la 8,0000 applications worldwide and thousands still in use which were manufactured in the 70 applications worldwid sands st and thousands still in use were man ations worldwide and thousands still in use which w were m nu u actur ffac e ’s, 80’s and 90’s, Rudolph Research Analytical has established itself as a premier vendor well known for its quality Analytical has establis a prem d itself as a premier vend nown for Analytical has established itself as a premier vendor well kn nown f s qu r it its , reliability and innovation. Rudolph’s entire line of instruments carry its exclusive 20 Y Rudolph’ ph’s ent f inst line of instrume rry it s entire line of instruments ca arry ry i excl ts e ear Service and Support Guarantee. Support Guarantee ort Gua ee. Rudolph Research Analytical of lph Research Analyt fers a comprehensive range of Preventive Maintenance and Service Programs Rudolph Research Analytical offers a comprehensive rang al offers a compreh e of Pre ge of P of ev ntiv ven . Rudolph has demonstrated a commitment to its customers by keeping installed instruments operational, not olph has demonstrate commitment to its c rs by ke Rudolph has demonstrated a commitment to its customeer y by eep k ng in pin only for 20 years, but in some cases for over 40 years. This long-term commitment to keeping our only for 20 years, but in some cases for over 40 years. Th for 20 years, but in so over 40 yea is long-t his lo on lon -term com erm instruments running makes the cost of ownership, over the life of a Rudolph Instrument, one of the lowest in the uments running ma e cost ersh wnership, the life instruments running makes the cost of ownership, over t r the lif o a Ru of f a laboratory market segment. At the date this document was published, there is no other laboratory ratory market segmen he t the date do his docum was publ laboratory market segment. At the date this document w blis ished, th h instrument manufacturer guaranteeing service and technical support for 20 years ument manufacturer ntee aranteeing ervice and t chnical instrument manufacturer guaranteeing service and tec ech ssuppor upp . The Rudolph Service Pledge: The The R Rudolph Service Pledge: e Rudolph Service Pledge: ce Pledge Earning your loyalty everyday E , through our commitment to exceptional service and attentive customer focu Earning your loyalty everyday, through our commitment to arning your loyalty everyday, through our comm Earning your loyalty everyday ryday, through our itm to excepti o exc o s . Integrity, Quality, and Innovation with a Global Reach. Integrity, Quality, and Innovation ntegrity, Qua nd In Integrity, Quality, and Innovation ty, and Innovat with w a with th a Globa G Gl Rudolph Research Analytical manufactures automatic Density Meters, Refractometers, Polarimeters, Saccharimeters and Rudolph Research An anufact ytical manufactures auto Density Rudolph Research Analytical manufactures automatic D Density M Mee ers, tter R Automation Solutions for a wide variety of industries. W ation Solutions for a wide variety of industries. Automation Solutions variety r a wide variety of indus ith over 8,000 laboratory instruments installed in demanding W th over Wit ith h ov over 8 00 la 8,0000 applications worldwide and thousands still in use which were manufactured in the 70 applications worldwid sands st and thousands still in use were man ations worldwide and thousands still in use which w were m nu u actur ffac e ’s, 80’s and 90’s, Rudolph Research Analytical has established itself as a premier vendor well known for its quality Analytical has establis a prem d itself as a premier vend nown for Analytical has established itself as a premier vendor well kn nown f s qu r it its , reliability and innovation. Rudolph’s entire line of instruments carry its exclusive 20 Y Rudolph’s entire line of instruments ca ph’s ent f inst line of instrume rry it arry ry i excl ts e ear Service and Support Guarantee. Support Guarantee ort Gua ee. Rudolph Research Analytical of lph Research Analyt fers a comprehensive range of Preventive Maintenance and Service Programs Rudolph Research Analytical of al offers a compreh e of Pre fers a comprehensive rangge of P of ev ntiv ven . Rudolph has demonstrated a commitment to its customers by keeping installed instruments operational, not olph has demonstrate commitment to its c rs by ke Rudolph has demonstrated a commitment to its customeer y by eep k ng in pin only for 20 years, but in some cases for over 40 years. This long-term commitment to keeping our for 20 years, but in so over 40 yea is long-t only for 20 years, but in some cases for over 40 years. Th his lo on lon -term com erm instruments running makes the cost of ownership, over the life of a Rudolph Instrument, one of the lowest in the uments running ma e cost ersh wnership, the life instruments running makes the cost of ownership, over t r the lif o a Ru of f a laboratory market segment. At the date this document was published, there is no other laboratory ratory market segmen he t the date do his docum was publ laboratory market segment. At the date this document w blis ished, th h instrument manufacturer guaranteeing service and technical support for 20 years ument manufacturer ntee aranteeing ervice and t chnical instrument manufacturer guaranteeing service and tec ech ssuppor upp . (Shown Center Left) Christina Says: Heidi Says: “Maximize your up time with a pre- “Our Customer support team is dedicated ventative maintenance plan designed to providing you with an exceptional for the way you work.” customer experience.” Rudolph stands behind each instrument purchase with a 20 year support guarantee. Rudolph is still repairing instruments it manufactured in the 1970’ Rudolph stands behind each instrument purchase s. with a 20 year support guarantee. Rudolph is still repairing instruments it manufactured in the 1970’s. Rudolph Research Analytical 55 Newburgh Road, Hackettstown, NJ 07840 USA • Phone: 973-584-1558 • Fax: 973-584-5440 • E-mail: info@rudolphresearch.com • Internet: www.rudolphresearch.com Specifications Features Autopol® V PLUS Autopol® VI Measuring Mode: Optical Rotation, Specific Rotation, Concentration & User-defined Scales Measuring Scale: Degrees Arc, % Concentration Measuring Range: ±89.9° Arc Optical Rotation, ±999.99° Arc Specific Rotation and 0-99.9% Concentration 0.001° Arc Optical Rotation 0.0001° Arc Optical Rotation Resolution 0.001% Concentration 0.0001% Concentration 0.001° Specific Rotation 0.0001° Specific Rotation 0.0001° Arc Optical Rotation USR Resolution 0.0001% Concentration Not Applicable 0.0001° Specific Rotation Repeatability: 0.002° Optical Rotation (OR) 0.0002° Optical Rotation (OR) (Between +1°– -1°) Standard Accuracy: 0.002ůp to 1° , 0.2% up to 5°, 0.01° above 5° (° in OR) High Accuracy Mode: Not Available 0.0003° Optical Rotation (OR) (Between +1°– -1°) Autopol V Plus Single: ±0.002° Arc over ±89.9° Arc. Autopol V Plus Six Wavelength (546nm and 589nm): AP High Accuracy Option ±0.002° over ±89.9° Arc. Not Applicable Accuracy for other wavelengths is the same as the standard model. Prism: Glan Thompson Calcite Quartz Optical Wavelengths: 365nm, 405nm, 436nm, 546nm, 589nm, 633nm (other wavelengths available) Wavelength Selection: Automatic by Touch Screen TempTrol™ Range: Automatic Electronic Heating & Cooling 10°-40°C TempTrol™ Accuracy: ±0.2°C Temp. Probe Range: 10°- 40°C Temp. Probe Accuracy: ±0.1°C Acid Resistance: Ceramic Quartz measurement cell and Nedox™ sample chamber (standard) Measurement Time: 4°/sec. slew rate and 5 sec. nominal settling time Light Source: Tungsten-halogen 6V, 20W, avg. 2,000 hour life Sample Chamber: Accepts sample tubes up to 200mm Data Storage/Internal Memory: 32 GB Non-removable Compact Flash Communication Interface: Touch Screen, 3 – USB Ports, 2 – RS232 Ports, Ethernet Port for Network Connection, Keyboard, Bar Code Scanner, Mouse, Network Capabilities Calibration: Automatic calibration by push-button Operating System Windows Embedded Display: 10.4 inch diagonal, 800-600 pixels, color, Flat Panel Monitor with Resistant Touch Screen Interface, 200 nits brightness, gasketted for spill protection User Interface: Touchscreen Measures samples with transmittance as Automatic Sensitivity Control: low as 0.01% (up to O.D. 4.0) Input Power: 85 – 260 VAC; 48 – 62 Hz, 150 – 200 Watts consumption Operating Dimensions: 32”W x 11.5”H x 18”D 81.28cm W x 29.21cm H x 45.72cm D Shipping Dimensions: 37”W x 24”H x 26”D 94cm W x 61cm H x 66cm D Operating Weight: 90 lbs. (41kg) Shipping Weight: 105 lbs. (48kg) Rudolph Research Analytical 55 Newburgh Road, Hackettstown, NJ 07840 USA • Phone: 973-584-1558 • Fax: 973-584-5440 • E-mail: info@rudolphresearch.com • Internet: www.rudolphresearch.com 3/2020